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The molecular structure of the corresponding product 3a was determined by X-ray crystallography (Figure 1, X-ray data for compound 3a: C23H23NO4, MW=377.42, T=274 (2) K, λ=0.71073 -Å, monoclinic space group, triclinic, P-1, a=9.369 (12, Å, b=10.308 (13, Å, c=10.606 (13, Å, α=94.23(2)°, β=95.71(2)°, γ=94.83(2)°, V=1012(2, Å-3, Z=2, ρcald=1.238 mg m-3, μ=0.085 mm-1, F(000)=400, crystal size 0.31x0.27x0.24 mm3, independent reflections 3639 [R(int)=0.0223, reflections collected 4753, refinement method, full-matrix least-squares on F2, goodness-of-fit on F2 1.013, final R indices [I> 2α(I, R1=0.0540, wR2=0.1361, R indices (all date) R 1=0.0986, wR2
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