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Volumn 351, Issue 1-2, 2009, Pages 141-146

One-pot synthesis of highly substituted allenylidene derivatives via palladium- or nickel-catalyzed tandem Michael addition-cyclization reaction

Author keywords

Allenes; Cyclization; Nickel; Palladium; Propargylic compounds

Indexed keywords


EID: 58549118934     PISSN: 16154150     EISSN: 15213897     Source Type: Journal    
DOI: 10.1002/adsc.200800582     Document Type: Article
Times cited : (20)

References (54)
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    • Ho, T.-L.1
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    • c) L. F. Tietze, F. Haunert, in: Stimulating Concepts in Chemistry, (Eds.: F. Vögtle, J. F. Stoddart, M. Shibasaki), Wiley-VCH, Weinheim, 2000, p 39;
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    • Tietze, L.F.1    Haunert, F.2
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    • For recent selected examples of metal-promoted tandem reactions, see: a
    • For recent selected examples of metal-promoted tandem reactions, see: a) K.-T. Yip, M. Yang, K.-L. Law, N.-Y. Zhu, D. Yang, J. Am. Chem. Soc. 2006, 128, 3130;
    • (2006) J. Am. Chem. Soc , vol.128 , pp. 3130
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  • 25
    • 19744369635 scopus 로고    scopus 로고
    • For some of the most recent typical reactions about allenes, see: a
    • For some of the most recent typical reactions about allenes, see: a) S.-S. Ng, T. F. Jamison, J. Am. Chem. Soc. 2005, 127, 7320;
    • (2005) J. Am. Chem. Soc , vol.127 , pp. 7320
    • Ng, S.-S.1    Jamison, T.F.2
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    • Eds, A.S.K. Hashmi, N. Krause, Wiley-VCH, Weinheim
    • h) A. S. K. Hashmi, in: Modern Allene Chemistry, (Eds.: A.S.K. Hashmi, N. Krause), Wiley-VCH, Weinheim, 2004, p 877.
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    • See Supporting Information for details
    • See Supporting Information for details.
  • 42
    • 58549106251 scopus 로고    scopus 로고
    • The molecular structure of the corresponding product 3a was determined by X-ray crystallography (Figure 1, X-ray data for compound 3a: C23H23NO4, MW=377.42, T=274 (2) K, λ=0.71073 -Å, monoclinic space group, triclinic, P-1, a=9.369 (12, Å, b=10.308 (13, Å, c=10.606 (13, Å, α=94.23(2)°, β=95.71(2)°, γ=94.83(2)°, V=1012(2, Å-3, Z=2, ρcald=1.238 mg m-3, μ=0.085 mm-1, F(000)=400, crystal size 0.31x0.27x0.24 mm3, independent reflections 3639 [R(int)=0.0223, reflections collected 4753, refinement method, full-matrix least-squares on F2, goodness-of-fit on F2 1.013, final R indices [I> 2α(I, R1=0.0540, wR2=0.1361, R indices (all date) R 1=0.0986, wR2
    • -3. CCDC 702185 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data-request/cif.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.