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For some recent examples of palladium-catalyzed reactions of propargylic carbonates with nucleophiles for the syntheses of 2-substituted benzofurans and indoles, in which nucleophiles attack on the less hindered carbon of the π-allylpalladium complex, see: (a) Yoshida, M, Morishita, Y, Fujita, M, Ihara, M. Tetrahedron Lett. 2004, 45, 1861
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For some recent examples of palladium-catalyzed reactions of propargylic carbonates with nucleophiles for the syntheses of 2-substituted benzofurans and indoles, in which nucleophiles attack on the less hindered carbon of the π-allylpalladium complex, see: (a) Yoshida, M.; Morishita, Y.; Fujita, M.; Ihara, M. Tetrahedron Lett. 2004, 45, 1861.
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33846286636
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Crystal data for 3ad have been deposited in CCDC as deposition number 620440: C21H24O6, MW, 372.40, T, 294(2) K, λ, 0.71073 Å, monoclinic space group, P1, a, 11.0511(10) Å, b, 20.5371(16) Å, c, 9.0441(8) Å, α, 90.00°, β, 96.047(4)°, γ, 90.00°, V, 2041.2(3) Å3, Z, 4, Dc, 1.212 mg/m3, μ, 0.088 mm-1, F(000, 816, crystal size 0.55 × 0.50 × 0.40 mm3, independent reflections 4008 [R (int, 0.0363, reflections collected 11295, refinement method, full-matrix least-squares on F2, goodness-of-fit on F 2 1.183, final R indices [I > 2σ(I, R1, 0.0977, wR2, 0.2172, R indices (all date) R1, 0.0603, wR2, 0.1856, exti
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For examples of π-allylpalladium complex and subsequent C-alkylation, see: Tsuji, J, Kobayashi, Y, Kataoka, H, Takahashi, T. Tetrahedron Lett. 1980, 21, 1475
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For examples of π-allylpalladium complex and subsequent C-alkylation, see: Tsuji, J.; Kobayashi, Y.; Kataoka, H.; Takahashi, T. Tetrahedron Lett. 1980, 21, 1475.
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For some examples of nucleophiles attack the more hindered side of the π-allylmetal complexes, see: a
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For some examples of nucleophiles attack the more hindered side of the π-allylmetal complexes, see: (a) Trost, B. M.; Hung, M.-H. J. Am. Chem. Soc. 1983, 105, 7757.
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