Use of a programmed temperature vaporizer and an in situ derivatization reaction to improve sensitivity in headspace-gas chromatography. Application to the analysis of chlorophenols in water

Journal of Chromatography A

Volumn 1216, Issue 7, 2009, Pages 1192-1199

  Pérez Pavón, José Luis ^a   Casas Ferreira, Ana María ^a   Fernández Laespada, María Esther ^a   Moreno Cordero, Bernardo ^a  

^a UNIVERSITY OF SALAMANCA   (Spain)

Author keywords

Derivatization; Headspace analysis; Low volatility compounds; Programmed temperature vaporizers

Indexed keywords

ACETIC ANHYDRIDES; ANALYTES; AQUEOUS MEDIUMS; CHLOROPHENOL; CHLOROPHENOLS; DERIVATIZATION; DERIVATIZATION REACTIONS; DICHLOROPHENOL; GLASS WOOLS; HEADSPACE; HEADSPACE ANALYSIS; IN-SITU; LOW LIMITS OF DETECTIONS; LOW-VOLATILITY COMPOUNDS; PROGRAMMED TEMPERATURE VAPORIZERS; S/N RATIOS; TRICHLOROPHENOL; VOLATILE COMPOUNDS;

ADSORPTION; CHEMICAL REACTIONS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; PHENOLS; VOLATILE ORGANIC COMPOUNDS; WATER ANALYSIS; WATER VAPOR;

GAS CHROMATOGRAPHY;

2 CHLOROPHENOL; 2,4 DICHLOROPHENOL; 2,4,6 TRICHLOROPHENOL; ACETIC ANHYDRIDE; CHLOROCRESOL; CHLOROPHENOL; VOLATILE AGENT; WATER;

ACCURACY; AQUEOUS SOLUTION; ARTICLE; CHEMICAL INTERACTION; DERIVATIZATION; GAS CHROMATOGRAPHY; METHODOLOGY; PRIORITY JOURNAL; TEMPERATURE; VAPORIZER; WATER ANALYSIS;

ANALYSIS OF VARIANCE; CHLOROPHENOLS; CHROMATOGRAPHY, GAS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TEMPERATURE; VOLATILE ORGANIC COMPOUNDS; WATER; WATER POLLUTANTS, CHEMICAL; WATER SUPPLY;

EID: 58249108686     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2008.12.034     Document Type: Article

References (28)

1. Kolb B. J. Chromatogr. A 842 (1999) 163
2. Lambropoulou D.A., Konstantinou I.K., and Albanis T.A. J. Chromatogr. A 1152 (2007) 70
3. Pérez Pavón J.L., del Nogal Sánchez M., Fernández Laespada M.E., and Moreno Cordero B. J. Chromatogr. A 1175 (2007) 106
4. Pérez Pavón J.L., del Nogal Sánchez M., Fernández Laespada M.E., García Pinto C., and Moreno Cordero B. J. Chromatogr. A 1141 (2007) 123
5. Kolb B., and Ettre L.S. Static Headspace-Gas Chromatography (2006), Wiley Interscience, Hoboken, NJ
6. Pérez Pavón J.L., del Nogal Sánchez M., Fernández Laespada M.E., and Moreno Cordero B. J. Chromatogr. A 1202 (2008) 196
7. Pérez Pavón J.L., Herrero Martín S., García Pinto C., and Moreno Cordero B. J. Chromatogr. A 1194 (2008) 103
8. Štajnbaher D., and Zupančič-Kralj L. J. Chromatogr. A 1190 (2008) 316
9. Heberer T., and Stan H.J. Anal. Chim. Acta 341 (1997) 21
10. Saraji M., and Bakhsi M. J. Chromatogr. A 1098 (2005) 30
11. Amijee M., Cheung J., and Wells R.J. J. Chromatogr. A 738 (1996) 43
12. Geibler A., and Schöler H.F. Water Res. 28 10 (1994) 2047
13. Turnes I., Rodriguez I., García C.M., and Cela R. J. Chromatogr. A 743 (1996) 283
14. Llompart M., Lourido M., Landín P., García-Jares C., and Cela R. J. Chromatogr. A 963 (2002) 137
15. Montero L., Conradi S., Weiss H., and Popp P. J. Chromatogr. A 1071 (2005) 163
16. In: Keith L.H. (Ed). Compilation of Sampling Analysis Methods (1991), US Environmental Protection Agency, Boca Raton, FL
17. Guidelines for Drinking Water Quality, 2nd ed., vol. 2, Health Criteria and Other Supporting Information, 1996, p. 940 and Addendum to vol. 2, 1998, p. 281, World Health Organization, Geneva.
18. Enhanced ChemStation, G1701CA, Version C00.00, Agilent Technologies, 1999, CA, United States.
19. Carey F.A., and Sundberg R.J. Advanced Organic Chemistry. Part A. Structure and Mechanisms. 4th ed. (2000), Kluwer Academic/Plenum Publishers
20. Dettmer K., and Engewald W. Anal. Bioanal. Chem. 373 (2002) 490
21. Coeur C., Jacob V., Denis I., and Foster P. J. Chromatogr. A 786 (1997) 185
22. Drechsel D., Dettmer K., Engewald W., Bittner Th., and Efer J. Chromatographia 54 (2001) 151
23. Vermeulen A., Welvaert K., and Vercammen J. J. Chromatogr. A 1071 (2005) 41
24. Fattahi N., Assadi Y., Hosseini M., and Jahromi E. J. Chromatogr. A 1157 (2007) 23
25. Rodriguez I., Turnes M.I., Mejuto M.C., and Cela R. J. Chromatogr. A 721 (1996) 297
26. Bianchi F., Careri M., Mucchino C., and Musci M. Chromatographia 55 (2002) 595
27. Quintana J., Rodil R., Muniategui-Lorenzo S., López-Mahía P., and Prada-Rodríguez D. J. Chromatogr. A 1174 (2007) 27
28. Ojala M., Ketola R., Virkki V., Sorsa H., and Kotiaho T. Talanta 44 (1997) 1253