Metal-ligand solution equilibria studied by electrospray ionization mass spectrometry: Effect of instrumental parameters

Journal of Mass Spectrometry

Volumn 44, Issue 1, 2009, Pages 120-127

  Di Marco, Valerio B ^a   Bombi, G Giorgio ^a   Zambon, Stefano ^a,b   Traldi, Pietro ^b  

^a UNIVERSITY OF PADOVA   (Italy)

^b CNR Consiglio Nazionale delle Ricerche   (Italy)

Author keywords

Aluminum; Complexes; ESI MS; Instrumental parameters; Solution equilibria

Indexed keywords

ALUMINA; ALUMINUM; DECOMPOSITION; DIMERS; DROP FORMATION; DROPS; DYES; FLOW RATE; GAS DYNAMICS; GASES; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION SOURCES; IONIZATION; IONIZATION OF GASES; IONS; LIGANDS; LIGHT METALS; MASS SPECTROMETERS; MASS SPECTROMETRY; METAL IONS; OLIGOMERS; PYROLYSIS; SPECTROMETERS; SPECTROMETRY; SPECTRUM ANALYSIS;

AQUEOUS SOLUTIONS; COMPLEXES; ELECTROSPRAY IONIZATION MASS SPECTROMETRIES; ESI-MS; GAS PHASE; INSTRUMENTAL PARAMETERS; MONOMERIC COMPLEXES; NEBULIZER GAS FLOW RATES; SODIUM IONS; SOLUTION FLOW RATES; SPECTRAL CHANGES; SURFACE ACTIVITIES; THERMAL DECOMPOSITIONS; TRANSFER EFFICIENCIES;

ELECTROSPRAY IONIZATION;

ALUMINUM; DIMER; LIGAND; METAL; MONOMER; PYRIDINE DERIVATIVE;

ANALYTIC METHOD; ARTICLE; DECOMPOSITION; ELECTROSPRAY MASS SPECTROMETRY; FLOW RATE; GAS; PRIORITY JOURNAL; SURFACE PROPERTY;

EID: 58249097239     PISSN: 10765174     EISSN: 10969888     Source Type: Journal    
DOI: 10.1002/jms.1481     Document Type: Article

References (21)

1. V. B. DiMarco, G. G. Bombi. Electrospraymass spectrometry (ESI-MS) in the study of metal-ligand solution equilibria. Mass Spectrometry Reviews 2006, 25, 347.
2. P. Kebarle, L. Tang. From ions in solution to ions in the gas phase - the mechanism of electrospray mass spectrometry. Analytical Chemistry 1993, 65, 972A.
3. H. J. Wang, G. R. Agnes. Evaluation of electrospray mass spectrometry as a technique for quantitative analysis of kinetically labile solution species. Analytical Chemistry 1999, 71, 3785.
4. L. Tang, P. Kebarle. Dependence of ion intensity in electrospray mass spectrometry on the concentration of the analytes in the electrosprayed solution. Analytical Chemistry 1993, 65, 3654.
5. E. Leize, A. Jaffrezic, A. VanDorsselaer. Correlation between solvation energies and electrospray mass spectrometric response factors. Study by electrospray mass spectrometry of supramolecular complexes in thermodynamic equilibrium in solution. Journal of Mass Spectrometry 1996, 31, 537.
6. 2+ and phenanthroline. Journal of Mass Spectrometry 2000, 35, 172.
7. T. L. Constantopoulos, G. S. Jackson, C. G. Enke. Effects of salt concentration on analyte response using electrospray ionization mass spectrometry. Journal of the American Society for Mass Spectrometry 1999, 10, 625.
8. P. J. R. Sjöberg, C. F. Bökman, D. Bylund, K. E. Markides. A method for determination of ion distribution within electrosprayed droplets. Analytical Chemistry 2001, 73, 23.
9. 2+ cations using electrospray ionization mass spectrometry and semiempirical PM5 methods. Journal of Molecular Structure 2007, 829, 111.
10. M. Franska. Electrospray ionization mass spectrometric study of platinum(II) complexes with nucleobases and dimethyl sulfoxide. International Journal of Mass Spectrometry 2007, 261, 86.
11. A. Schmidt, M. Karas, T. Dülcks. Effect of different solution flow rates on analyte ion signals in nano-ESI MS, or: when does ESI turn into nano-ESI? Journal of the American Society for Mass Spectrometry 2003, 14, 492.
12. K. Benkestock, G. Sundqvist, P. O. Edlund, J. Roeraade. Influence of droplet size, capillary-cone distance and selected instrumental parameters for the analysis of noncovalent protein-ligand complexes by nano-electrospray ionization mass spectrometry. Journal of Mass Spectrometry 2004, 39, 1059.
13. J. Fernandez de la Mora, I. G. Loscertales. The current emitted by highly conducting Taylor cones. Journal of Fluid Mechanics 1994, 260, 155.
14. R. J. Pfeifer, C. D. Hendricks Jr. Parametric studies of electrohydrodynamic spraying. AIAA Journal 1968, 6, 496.
15. J. B. Fenn, M. Mann, C. K. Meng, S. F. Wong, C. M. Whitehouse. Electrospray ionization - principles and practice. Mass Spectrometry Reviews 1990, 9, 37.
16. V. B. Di Marco, G. G. Bombi, A. Tapparo, A. K. Powell, C. E. Anson. Complexation of aluminium(III) with 3-hydroxy-2(1H)-pyridinone. Solution state study and crystal structure of tris(3-hydroxy-2(1H)-pyridinonato) aluminium(III). Journal of the Chemical Society, Dalton Transactions 1999, 2427.
17. V. DiMarco, G. G. Bombi, M. Tubaro, P. Traldi. Electrospray ionization mass spectrometry in studies of aluminium(III)-ligand solution equilibria. Rapid Communications in Mass Spectrometry 2003, 17, 2039.
18. V. B. Di Marco, G. G. Bombi, M. Ranaldo, P. Traldi. Surface-activated chemical ionization versus electrospray ionization in the study of selected aluminium(III)/ligand solution equilibria. Rapid Communications in Mass Spectrometry 2006, 20, 710.
19. V. B. Di Marco, G. G. Bombi, M. Ranaldo, P. Traldi. Metal-ligand solution equilibria studied by electrospray ionization mass spectrometry: correlation between ion intensity and acid-base equilibria in solution. Rapid Communications in Mass Spectrometry 2007, 21, 3825.
20. W. H. Press, B. P. Flannery, S. A. Teukolsky, W. T. Vetterling. Numerical Recipes: The Art of Scientific Computing. Cambridge University Press: Cambridge, 1986.
21. A. F. Cotton, G. Wilkinson, C. A. Murillo, M. Bochmann. Advanced Inorganic Chemistry. John Wiley & Sons: New York, 1999.