Enhanced detection of sphingoid bases via divalent ruthenium bipyridine complex derivatization and electrospray ionization tandem mass spectrometry

Analytical Chemistry

Volumn 81, Issue 1, 2009, Pages 495-502

  Masood, M Athar ^a   Xu, Xia ^a   Acharya, Jairaj K ^b   Veenstra, Timothy D ^a   Blonder, Josip ^a  

^a SAIC FREDERICK INC   (United States)

^b NATIONAL CANCER INSTITUTE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AMINO GROUPS; ANALYTES; BIPYRIDINE; CELL EXTRACTS; DERIVATIZATION; DIHEXAFLUOROPHOSPHATE; IN CELLS; IONIZATION EFFICIENCIES; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRIES; RUTHENIUM BIPYRIDINE; RUTHENIUM COMPLEXES; RUTHENIUM IONS; SPHINGANINE; SPHINGOID BASIS; SPHINGOLIPIDS; SPHINGOMYELINS; SPHINGOSINE; TANDEM MASS SPECTROMETRIES;

AMINES; CHROMATOGRAPHIC ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IONIZATION; IONIZATION OF LIQUIDS; IONIZATION POTENTIAL; LIQUID CHROMATOGRAPHY; MASS SPECTROMETERS; MASS SPECTROMETRY; RUTHENIUM; RUTHENIUM COMPOUNDS; SPECTROMETERS; SPECTROMETRY; SPECTRUM ANALYSIS;

ELECTROSPRAY IONIZATION;

2,2'-DIPYRIDYL; CHROMATOGRAPHY, LIQUID; ORGANOMETALLIC COMPOUNDS; RUTHENIUM; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; SPHINGOLIPIDS; SPHINGOSINE; TANDEM MASS SPECTROMETRY;

EID: 58149477897     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac8019043     Document Type: Article

References (25)

1. Barenholz, Y.; Thompson, T. E. Chem Phys. Lipids 1999, 102, 29-34.
2. Raghavendra, P. H.; Yuan, C.; Allegood, J. C.; Edwards, M. B.; Wang, X.; Acharya, U.; Acharya, J. K. Proc. Natl. Acad. Sci. U.S.A. 2007, 104, 11364-11369.
3. Fyrst, H.; Zhang, X.; Herr, D. R.; Byun, H. S.; Bittman, R.; Phan, V. H.; Harris, G. L.; Saba, J. D. J. Lipid Res. 2008, 49, 597-606.
4. Dennis, R. D.; Wiegandt, H. Adv. Lipid Res. 1993, 26, 321-351.
5. Hildebrandt, H.; Jonas, U.; Ohashi, M.; Klaiber, I.; Rahmann, H. Comp. Biochem. Physiol., B 1999, 122, 83-88.
6. Kolesnick, R.; Fuks, Z. J. Exp. Med. 1995, 181, 1949-1952.
7. Huwiler, A. T.; Kolter, J.; Pfeilschifter, J.; Sandhoff, K. Biochim. Biophys. Acta 2000, 1485, 63-99.
8. Hannun, Y. A.; Obeid, L. M. J. Biol. Chem. 2002, 277, 25847-25850.
9. Helms, J.; Zurzolo, C. Traffic 2004, 5, 247-254.
10. Mathias, M.; Kolesnick, R. Adv. Lipid Res. 1993, 25, 65.
11. Pyne, S.; Pyne, N. J. Biochem. J. 2000, 349, 385-402.
12. Merrill, A. H., Jr.; Sullards, M. C.; Wang, E.; Voss, K. A.; Riley, R. T. Environ. Health Perspect. 2001, 109 (Suppl. 2), 283-289.
13. Prieschl, E. E.; Baumruker, T. Immunol. Today 2000, 21, 555-560.
14. Herr, D. R. H.; Fyrst, V.; Phan, K.; Heinecke, R.; Georges, G. L.; Harris, G.; Saba, J. D. Development 2003, 130, 2443-2453.
15. Acharya, J. K.; Dasgupta, U.; Rawat, S. S.; Yuan, C.; Sanxaridis, P. D.; Yonamine, I.; Karim, P.; Nagashima, K.; Brodsky, M. H.; Tsunoda, S.; Acharya, U. Neuron 2008, 57, 69-79.
16. Ma, D. W. Appl. Physiol. Nutr. Metab. 2007, 32, 341-350.
17. Sullards, M. C.; Allegood, J. C.; Kelly, S.; Wang, E.; Haynes, C. A.; Park, H.; Chen, Y.; Merrill, A. H., Jr. Methods Enzymol. 2007, 432, 83-115.
18. Merrill, A. H., Jr.; Sullards, M. C.; Allegood, J. C.; Kelly, S.; Wang, E. Methods 2005, 36, 207-224.
19. Sullards, M. C.; Merrill, A. H., Jr. Sci. STKE 2001, 67, 1-11, see Figure 6 in this reference.
20. Caligan, T. B.; Peters, K.; Ou, J.; Wang, E.; Saba, J.; Merrill, A. H., Jr. Anal. Biochem. 2000, 281, 36-41.
21. Fyrst, H.; Herr, D. R.; Harris, G. L.; Saba, J. D. J. Lipid Res. 2004, 45, 54-62.
22. Bartolome, A.; Bardliving, C.; Rao, G.; Tolosa, L. Anal. Biochem. 2005, 345, 133-139.
23. Staffilani, M.; Höss, E.; Giessen, U.; Schneider, E.; Hartl, F.; Josel, H. P.; De Cola, L. Inorg. Chem. 2003, 42 (23), 7789-7798.
24. Ciana, L. D.; Hamachi, I.; Meyer, T. J. J. Org. Chem. 1989, 54, 1731-1735.
25. Sullards, C. Methods Enzymol. 2000, 312, 32-45.