SCOPUS 정보 검색 플랫폼

Volumn 5, Issue 6, 2008, Pages 490-494

Oxalic acid dihydrate: A reusable and cost-effective catalyst for the synthesis of bis(indolyl)methanes under solvent-free conditions

(5) Dabiri, Minoo a Baghbanzadeh, Mostafa a Azimi, Seyedeh C a Ahmadzadeh Asl, Shaghayegh a Ardestani, Reza R a

a SHAHID BEHESHTI UNIVERSITY (Iran)

Author keywords

Heterocycles; Indole; Oxalic acid; Solvent free

Indexed keywords

EID: 57349192204 PISSN: 15701786 EISSN: None Source Type: Journal
DOI: 10.2174/157017808785740516 Document Type: Article

Times cited : (8)

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- Melting points were measured on an Elecrtothermal 9100 apparatus and are uncorrected. Mass spectra were recorded on a FINNIGANMAT 8430 mass spectrometer operating at an ionization potential of 70 eV. 1H and 13C NMR spectra were recorded on a BRUKER DRX-300 AVANCE spectrometer at 300.13 and 75.47 MHz, respectively. IR spectra were recorded on a Bomem MB-Series FTIR spectrophotometer. General procedure for the synthesis of BIMs: Aldehyde or ketone (2 mmol, and indole derivative (1 mmol) were mixed with (COOH)2 2H2O (0.05 mmol) and placed in a round bottomed flask. The mixture was stirred at ambient temperature. After the completion of the reaction confirmed by TLC eluent: n-hexane/ethyl acetate: 3/1, cold H2O was added to the mixture and the precipitated product was separated by simple filtration. Finally, the crude product was recrystallized from ethyl acetate/n-hexane or ethanol. All of the products are known and c
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