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Crystal data for 2b. C24H13Cl 3O2S, M, 471.75, triclinic, space group P-1, a, 7.605(10)Å, b, 10.382(9)Å, c, 14.031(10)Å, V, 1053.9(9)Å3, Z, 2, f (000, 480, μ, 0.553mm-1, Dc, 1.487 mg/m3. The reflections collected were 4603 of which 3682 unique [R (int, 0.0239, 1977 reflections I > 2σ(I, R1, 0.0444 and wR2, 0.1204 for 1977[I > 2σ(I, R1, 0.1042 and wR 2, 0.1823 for all (3682) intensity data. Goodness-of-fit 1.008, residual electron density in the final Fourier map was 0.289 and -0.331 e Å-3. Complete crystallographic data, as a CIF file, have been deposited with the Cambridge Crystallographic Data Centre CCDC number is 646678
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-3. Complete crystallographic data, as a CIF file, have been deposited with the Cambridge Crystallographic Data Centre (CCDC number is 646678).
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27144434946
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Miyahara, Y.; Inazu, T.; Yoshino, T. Bull. Chem. Soc. Jpn. 1980, 53, 1187-1188.
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(1980)
Bull. Chem. Soc. Jpn
, vol.53
, pp. 1187-1188
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Miyahara, Y.1
Inazu, T.2
Yoshino, T.3
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