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C. Möllers, J. Prigge, B. Wibbeling, R. Fröhlich, A. Brockmeyer, H. J. Schäfer, E. Schmälzlin, C. Bräuchle, K. Meerholz, E.-U. Würthwein, Eur. J. Org. Chem. 2003, 1198-1208.
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56749105464
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Data sets were collected with Enraf Nonius CAD4 and Nonius KappaCCD diffractometers, in case of Mo radiation equipped with a rotating anode generator. Programs used: data collection EXPRESS (Nonius B. V., 1994) and COLLECT (Nonius B. V., 1998), data reduction MolEN (K. Fair, Enraf-Nonius B. V., 1990) and Denzo-SMN (Z. Otwinowski, W. Minor, Methods Enzymol. 1997, 276, 307-326)
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Data sets were collected with Enraf Nonius CAD4 and Nonius KappaCCD diffractometers, in case of Mo radiation equipped with a rotating anode generator. Programs used: data collection EXPRESS (Nonius B. V., 1994) and COLLECT (Nonius B. V., 1998), data reduction MolEN (K. Fair, Enraf-Nonius B. V., 1990) and Denzo-SMN (Z. Otwinowski, W. Minor, Methods Enzymol. 1997, 276, 307-326)
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17
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0038414570
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and Denzo (Z. Otwinowski, D. Borek,W. Majewski, W. Minor, Acta Crystallogr., Sect. A 2003, 59, 228-234),
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and Denzo (Z. Otwinowski, D. Borek,W. Majewski, W. Minor, Acta Crystallogr., Sect. A 2003, 59, 228-234),
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18
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84943920736
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structure solution SHELXS-97 (G. M. Sheldrick, Acta Crystallogr., Sect. A 1990, 46, 467-473),
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structure solution SHELXS-97 (G. M. Sheldrick, Acta Crystallogr., Sect. A 1990, 46, 467-473),
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19
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37549039510
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structure refinement SHELXL-97 (G. M. Sheldrick, Acta Crystallogr., Sect. A 2008, 64, 112-122),
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structure refinement SHELXL-97 (G. M. Sheldrick, Acta Crystallogr., Sect. A 2008, 64, 112-122),
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20
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56749176264
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graphics SCHAKAL (E. Keller, 1997, CCDC-694201 (for 5d, 694202 (for 5f, 694203 (for 3a·CoCl2, 694204 (for 3a·ZnBr2, 694205 (for 3b·ZnBr2, 694206 (for 3b·CuCl 2, 694207 [for 4b·Ni(ClO4) 2, 694208 (for 4g, 694209 [for 4d·Ni(NO 3)2, 694210 (for 6b, 694211 [for 7a·Ni(ClO4)2, 694212 [for 6·Ni(NO3)2, 694213 (for 4h, 694214 [for 4h·Ni(NO3)2, 694215 (for 6·2PdCl2, 694348 (for 4b) and -697731 (for 1d) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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2) -694348 (for 4b) and -697731 (for 1d) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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