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Volumn 47, Issue 21, 2008, Pages 9733-9735

A unique Mn2Gd2 tetranuclear compound of p-tert-butylthiacalix[4]arene

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EID: 56649117426     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic801086n     Document Type: Article
Times cited : (42)

References (30)
  • 26
    • 56649101190 scopus 로고    scopus 로고
    • Crystal data for 1: C94. 04H 148.94Gd2Mn2O25.43S8, M, 2367.41 g mol-1, monoclinic, C2/c, a, 35.358(5) Å b, 14.627(5) Å, c, 45.311(5) A, α, 90.00°, β, 96.543(5)°, γ, 90.00°, V, 23281(9) Å3, Z, 8, Dcalcd, 1.351 g cm-3, μ, 1.543 mm-1, T, 150(2) K, θmax, 25.0°, F(000, 9781, crystal dimensions 0.22 x 0.16 x 0.15 mm 3, reflections collected/unique, 77 489/20 527 (R int, 0.0470, final R1, 0.0549, wR2, 0.1466 [I > 2σ(I, GOF, 1.06. The X-ray intensity data for compound 1 were collected on a Bruker SMART APEX CCD diffractometer with graphite- monochromatized Mo Kα radiation (λ, 0.710 73 Å) operated at 2.0 kW 50 kV, 40 mA, The crystal
    • 19 All of the non-hydrogen atoms were refined anisotropically except some isolated molecular atoms, which were refined without hydrogen atoms. See the Supporting Information for further details. CCDC reference number 698364. The atomic coordinates for this structure have been deposited with the Cambridge Crystallographic Data Centre. The coordinates can be obtained, upon request, from the Director, Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, U.K.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.