Organization of tetrahedral chalcogenide clusters using a tetrahedral quadridentate linker

Inorganic Chemistry

Volumn 47, Issue 21, 2008, Pages 9724-9726

  Zhang, Qichun ^a   Bu, Xianhui ^b   Lin, Zhien ^a   Wu, Tao ^a   Feng, Pingyun ^a  

^a UNIVERSITY OF CALIFORNIA   (United States)

^b CALIFORNIA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 56649105117     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic800588q     Document Type: Article

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28. 2 using SHELXL-97. The high R factor for MCOF-10 is due to the low quality of the crystal that limits the diffraction angle to only 35° and an overall weak diffraction. This phenomenon is common in chalcogenide structures with large clusters, C1 in this case. Repeated syntheses and crystal data collection fail to improve the data quality.