Novel concentration-driven structural interconversion in shape-specific solids supported by the octahedral [Re6(μ3-Se)8]2+ cluster core

Inorganic Chemistry

Volumn 41, Issue 24, 2002, Pages 6175-6177

  Selby, Hugh D ^a   Orto, Peter ^a   Carducci, Michael D ^a   Zheng, Zhiping ^a  

^a University of Arizona   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CADMIUM; POLYMER; RHENIUM; SELENIUM DERIVATIVE;

ARTICLE; BIOTRANSFORMATION; CHEMICAL MODIFICATION; CHEMICAL STRUCTURE; CONCENTRATION (PARAMETERS); CRYSTALLOGRAPHY; POLYMERIZATION; SOLID STATE; STRUCTURE ANALYSIS; TWO HYBRID SYSTEM;

EID: 0037011005     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic025925p     Document Type: Article

References (31)

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27. 2O in methanol was added. Diffusion with diethyl ether resulted in red plate-shaped crystals of 3 in quantitative yields.
28. 3/cell. From this point on, atoms in the region were removed, and the solvent region was refined as a diffuse contribution without specific atom positions using the Platon module SQUEEZE (van der Sluis, P.; Spek, A. L. Acta Crystallogr. 1990, A46, 194.). The solvent contribution amounted to 252 electrons per cell. Data for both structures were collected using a Bruker SMART 1000 CCD based area detector diffractometer with graphite monochromated Mo Kα (λ = 0.71073 Å) radiation. Structures were solved with direct methods followed by Fourier synthesis using Bruker's SHELXTL (v. 5.0) software package.
29. 3/cell. From this point on, atoms in the region were removed, and the solvent region was refined as a diffuse contribution without specific atom positions using the Platon module SQUEEZE (van der Sluis, P.; Spek, A. L. Acta Crystallogr. 1990, A46, 194.). The solvent contribution amounted to 252 electrons per cell. Data for both structures were collected using a Bruker SMART 1000 CCD based area detector diffractometer with graphite monochromated Mo Kα (λ = 0.71073 Å) radiation. Structures were solved with direct methods followed by Fourier synthesis using Bruker's SHELXTL (v. 5.0) software package.
30. 3/cell. From this point on, atoms in the region were removed, and the solvent region was refined as a diffuse contribution without specific atom positions using the Platon module SQUEEZE (van der Sluis, P.; Spek, A. L. Acta Crystallogr. 1990, A46, 194.). The solvent contribution amounted to 252 electrons per cell. Data for both structures were collected using a Bruker SMART 1000 CCD based area detector diffractometer with graphite monochromated Mo Kα (λ = 0.71073 Å) radiation. Structures were solved with direct methods followed by Fourier synthesis using Bruker's SHELXTL (v. 5.0) software package.
31. 3/cell. From this point on, atoms in the region were removed, and the solvent region was refined as a diffuse contribution without specific atom positions using the Platon module SQUEEZE (van der Sluis, P.; Spek, A. L. Acta Crystallogr. 1990, A46, 194.). The solvent contribution amounted to 252 electrons per cell. Data for both structures were collected using a Bruker SMART 1000 CCD based area detector diffractometer with graphite monochromated Mo Kα (λ = 0.71073 Å) radiation. Structures were solved with direct methods followed by Fourier synthesis using Bruker's SHELXTL (v. 5.0) software package.