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note
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2: C, 68.82; H, 6.42; N, 5.95.
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26
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56449123065
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note
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2. Further details concerning data collection and refinement are given in Ref. [25].
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27
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56449119668
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note
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2 = 0.0839; Largest diff. peak and hole 0.342 and -0.464 e Å-3.
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28
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56449123367
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note
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3 (2 mmol) dioxane (3 mL) were combined in a small Schlenk tube under argon and the mixture was heated at 80 °C for 5 h. At the end of the reaction, the mixture was cooled and volatiles were removed under vacuum. The product was extracted with diethyl ether, filtered through a pad of silicagel with copious washings, concentrated, and purified by flash chromatography on silicagel. The purity of the compounds was checked by NMR and yields are based on arylchloride.
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35
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18844393165
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