Simplifying the complex1H NMR spectra of fluorine-substituted benzamides by spin system filtering and spin-state selection: Multiple-quantum-single-quantum correlation

Journal of Physical Chemistry A

Volumn 112, Issue 42, 2008, Pages 10526-10532

  Baishya, Bikash ^a   Manjunatha Reddy, G N ^a   Prabhu, Uday Ramesh ^a   Guru Row, T N ^a   Suryaprakash, N ^a  

^a INDIAN INSTITUTE OF SCIENCE   (India)

Author keywords

[No Author keywords available]

Indexed keywords

AROMATIC COMPOUNDS; COUPLINGS; FLUORINE; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC POLYMERS; PROTONS;

AROMATIC RINGS; BENZAMIDES; COMPLEX 1; HETERONUCLEAR COUPLINGS; HOMONUCLEAR COUPLINGS; PHENYL RINGS; PROTON NMR; QUANTUM CORRELATIONS; SCALAR COUPLINGS; SPIN STATES; SPIN SYSTEMS;

SPIN DYNAMICS;

BENZAMIDE DERIVATIVE; FLUORINE; PROTON;

ARTICLE; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; QUANTUM THEORY; STANDARD;

BENZAMIDES; FLUORINE; MAGNETIC RESONANCE SPECTROSCOPY; PROTONS; QUANTUM THEORY; REFERENCE STANDARDS;

EID: 55649106515     PISSN: 10895639     EISSN: None     Source Type: Journal    
DOI: 10.1021/jp8055174     Document Type: Article

References (32)

1. Günther, H. NMR Spectroscopy, Basic Principles, Concepts, and Applications in Chemistry; John Wiley & Sons: New York, 1992.
2. Ernst, R. R.; Bodenhausen, G.; Wokaun, A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions; Clarendon Press: Oxford, U.K., 1991.
3. Keeler, J. Understanding NMR Spectroscopy; John Wiley & Sons: Chichester, England, 2005.
4. Jeener, J. Ampere Summer School, Basko Polje, Yugoslavia, 1971.
5. Aue, W. S.; Bartholdi, E.; Ernst, R. R. J. Chem. Phys. 1976, 64, 2229-2246.
6. Bachmann, S.; Aue, W. F.; Müller, L.; Ernst, R. R. J. Magn. Reson. 1977, 28, 29-39.
7. Nagayama, K.; Bachmann, P.; Wüthrich, K; Ernst, R. R. / Magn. Reson. 1978, 31, 133-148.
8. Macura, S.; Brown, L. R. J. Magn. Reson. 1983, 53, 529-535.
9. Shaka, A. J.; Keeler, J.; Freeman, R. J. Magn. Reson. 1984, 56, 294-313.
10. Neuhaus, D.; Wagner, G.; Vašàk, M.; Käegi, J. H. R.; Wüthrich, K. Eur. J. Biochem. 1985, 151, 257-273.
11. Kay. L. E.; Bax, A. J. Magn. Reson. 1990, 86, 110-126.
12. Heikkinen, S.; Aitio, H.; Permi, P.; Folmer, R.; Lappalainen, K.; Kilpeläinen. I. J. Magn. Reson. 1999. 137, 243-246.
13. Bax, A.; Max, D.; Zax, D. J. Am. Chem. Soc. 1992, 114, 6923-6925.
14. Reif, B.; Köck, M.; Kerssebaum, R.; Schleuchcr, J.; Gritsinger, C. J. Magn. Reson., B 1996, 112, 295-301.
15. Hu, J. S.; Bax, A. J. Am. Chem. Soc. 1997, 119, 6360-6368.
16. Oschkinat, H.; Pastore, A.; Pfändler, P.; Bodenhausen, G. J. Magn. Reson. 1986, 69, 559-566.
17. Brüsehweiler. R.; Madsen, J. C.; Griesinger, C.; Sørensen, O. W.; Ernst, R. R. J. Magn. Reson. 1987, 73, 380-385.
18. Bax, A.; Freeman, R. J. Magn. Reson. 1981, 44, 542-561.
19. Griesinger, C.; Sørensen, O. W.; Ernst, R. R. J. Chem. Phys. 1986, 85, 6837-6852 .
20. Pfändler, P.; Bodenhausen, G. J. Magn. Reson. 1987, 72, 475-492.
21. Montelione, G. T.; Winkler, M. E.; Rauenbuehler, P.; Wagner, G. J. Magn. Reson. 1989, 82, 198-204.
22. Sørensen, O. W. J. Magn. Reson. 1990, 90, 433-438.
23. Griesinger, C.; Sørensen, O. W.; Ernst, R. R. Two-dimensional correlation of connected NMR transitions. J. Am. Chem. Soc. 1985, 107, 6394-6396.
24. Eggenbrrger, U.; Karimi-Nejad, Y.; Thüring, H.; Rüterjans, H.; Griesinger, C. J. Biomol. NMR 1992, 2, 583-590.
25. Schmidt, J. M.; Ernst, R. R.; Aimoto, S.; Kainosho, M. J. Biomol. NMR 1995, 6, 95-105.
26. Bikash, B.; Suryaprakash, N. J. Phys. Chem. A 2007, 111, 5211-5217.
27. Bikash, B.; Suryaprakash, N. J. Chem. Phys. 2007, 127, 214510.
28. Caliendo, G.; Santagada, V.; Perissutti, E.; Severino, B.; Fiorino, F.; Warner, T. D.; Wallace, J. L.; Ifa, D. R.; Antunes, E.; Cirino, G.; de Nucci, G. Eur. J. Med. Chem. 2001, 36, 517-530.
29. Levitt, M. H.; Ernst, R. R. Chem. Phys. Lett. 1983, 100, 119-123.
30. Levitt, M. H.; Ernst, R. R. J. Chem. Phys. 1985, 83, 3297-3310.
31. Chopra, D.; Guru Row., T. N. Cryst. Eng. Commun. 2008, 10, 54-67.
32. Diehl, P.; Kellerhals, H. P.; Niederberger, W. J. Magn. Reson. 1971, 4, 352-357.