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Reactions reported in ref. 7a required oxygen atmosphere to minimize competing ethyl addition, and the authors noted significant hazards associated with that procedure
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(b) Reactions reported in ref. 7a required oxygen atmosphere to minimize competing ethyl addition, and the authors noted significant hazards associated with that procedure.
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2 Preliminary tests show that the pure (Z)-hydrazone leads to the same diastereomer, suggesting in situ isomerization of the C-N bond. This point is still under investigation.
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