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One could also envisage that the formation of the saturated cluster 24, rather than the fluorenyl analogue of the alcohol 15, may have occurred by dehydration, as from 15 to 11, and subsequent hydrogenation through reaction of the acid with cobalt-containing decomposition products.
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66
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Crystal data for 24: C24H11Co 3O9, MI=620.12, monoclinic, space group P2 1/n, 14, a, 8.702(6, 6, 30.56(2, c, 26.752(19) Å, β= 98.679(12)°, V=7032(9) Å3, Z, 12, ρcalcd 1.757 g cm3, μ, 2.151 mm-1, 7=173 K, R1, 0.1098
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