Large-scale synthesis of water soluble non-ionic dendrons by stepwise extraction purifications

Macromolecular Rapid Communications

Volumn 29, Issue 21, 2008, Pages 1758-1763

  Kim, Hyun Yu ^a   Lee, Byung Ill ^a   Cho, Byoung Ki ^a  

^a Dankook University   (South Korea)

Author keywords

Extraction purifications; Hydrophilic polymers; Large scale synthesis; Molecular weight distribution; Water soluble non ionic dendrons

Indexed keywords

ABS RESINS; BUILDING MATERIALS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; COLLOIDS; DENDRIMERS; ELECTRIC CONDUCTIVITY; ETHYLENE; GELATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHILICITY; IONIC LIQUIDS; IONIZATION OF LIQUIDS; MASS SPECTROMETRY; MOLECULAR WEIGHT; MOLECULAR WEIGHT DISTRIBUTION; POLYETHYLENE OXIDES; POLYMERS; PURIFICATION; SOLVENT EXTRACTION;

BUILDING BLOCKS; DENDRONS; DRUG CARRIERS; HYDROPHILIC POLYMERS; IONIC CONDUCTORS; LARGE-SCALE SYNTHESIS; NARROW MOLECULAR WEIGHT DISTRIBUTIONS; POLY(ETHYLENE OXIDE); POLYETHER DENDRONS; REACTION YIELDS; SECOND GENERATIONS; SOFT MATERIALS; STRAIGHTFORWARD METHODS; SYNTHESIS OF; SYNTHESIS PROCEDURES; SYNTHETIC STEPS;

COLUMN CHROMATOGRAPHY;

EID: 55349149678     PISSN: 10221336     EISSN: 15213927     Source Type: Journal    
DOI: 10.1002/marc.200800415     Document Type: Article

References (28)

1. [la] J. F. G. A. Jansen, E. M. M. de Brabander-van den Berg, E. W. Meijer, Science 1994, 266, 1226;
2. [1b] S. Fuchs, H. Otto, S. Jehle, P. Henklein, A. D. Schlüter, Chem. Commun. 2005, 1830;
3. [1c] N. Malik, R. Wiwattanapatapee, R. Klopsch, K. Lorenz, H. Frey, J. W. Weener, E. W. Meijer, W. Paulus, R. Duncan, J. Controlled Release 2000, 65, 133;
4. [1d] C. C. Lee, M. Yoshida, J. M. J. Fréchet, E. E. Dy, F. C. Szoka, Bioconjugate Chem. 2005, 26, 535;
5. [1e] R. J. Amir, D. Shabat, Chem. Commun. 2004, 1614.
6. [2a] G. Caminati, N. I Turro, D. A. Tomalia, J. Am. Chem. Soc. 1990, 112, 8515;
7. [2b] G. R. Newkome, C. N. Moorefield, G. R. Baker, M. J. Saunders, S. H. Grossman, Angew. Chem., Int. Ed. Engl. 1991, 30, 1178;
8. [2c] C. J. Hawker, K. L. Wooley, J. M. J. Fréchet, J. Chem. Soc., Perkin Trans. 1 1993, 1287;
9. [2d] C. Cheng, M. Schmidt, A. Zhang, A. D. Schlüter, Macromolecules 2007, 40, 220.
10. P. R. Ashton, S. E. Boyd, C. L. Brown, N. Jayaraman, J. F. Stoddart, Angew. Chem., Int. Ed. 1997, 36, 732.
11. [4a] L. Tian, P. T. Hammond, Chem. Mater. 2006, 28, 3976;
12. [4b] M. Berna, D. Dalzoppo, G. Pasut, M. Manunta, L. Izzo, A. T. Jones, E. Duncan, F. M. Veronese, Biomacromolecules 2006, 7, 146;
13. [4c] X. Feng, D. Taton, R. Borsali, E. L. Chaikof, Y. Gnanou, J. Am. Chem. Soc. 2006, 128, 11551;
14. [4d] S. M. Grayson, J. M. J. Fréchet, J. Am. Chem. Soc. 2000, 122, 10335;
15. [4e] E. R. Gillies, J. M. J. Fréchet, J. Am. Chem. Soc. 2002, 224, 14137.
16. H. Ihre, O. L. Padilla De Jesús, J. M. J. Fréchet, J. Am. Chem. Soc. 2001, 123, 5908.
17. [6a] M. Jayaraman, J. M. J. Fréchet, J. Am. Chem. Soc. 1998, 220, 12996;
18. [6b] Y.-W. Chung, J.-K. Lee, W.-C. Zin, B.-K. Cho, J. Am. Chem. Soc. 2008, 230, 7139;
19. [6c] Y.-W. Chung, B.-I. Lee, H.-Y. Kim, U. Wiesner, B.-K. Cho, J. Polym. Sci., Part A: Polym. Chem. 2007, 45, 4988.
20. F. Wurm, J. Nieberle, H. Frey, Macromolecules 2008, 41, 1909.
21. [8a] K.-S. Moon, H.-J. Kim, E. Lee, M. Lee, Angew. Chem., Int. Ed. 2007, 46, 6807;
22. [8b] S. V. Aathimanikandan, E. N. Savariar, S. Thayumanavan, J. Am. Chem. Soc. 2005, 127, 14922.
23. [9a] Z. Bo, J. P. Rabe, A. D. Schlüter, Angew. Chem., Int. Ed. 1999, 38, 2370;
24. [9b] Z. Bo, C. Zhang, N. Severin, I. P. Rabe, A. D. Schlüter, Macromolecules 2000, 33, 2688;
25. [9c] G. R. Newkome, K. K. Kotta, A. Mishra, C. N. Moorefield, Macromolecules 2004, 37, 8262;
26. [9d] R. S. Dhanikula, P. Hildgen, Bioconjugate Chem. 2006, 17, 29;
27. [9e] D.-J. Hong, E. Lee, M. Lee, Chem. Commun. 2007, 1801;
28. [9f] W. Li, A. Zhang, A. D. Schlüter, Macromolecules 2008, 41, 43.