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3 (0.5mL) with a 5% aqueous solution of sodium citrate (0.5 mL). The capillaries were filled with the mixture, capped at both ends and left to develop at room temperature for another 30 min, After rinsing with acetone, the capillaries were calcinated at 400 °C before use.
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3 (0.5mL) with a 5% aqueous solution of sodium citrate (0.5 mL). The capillaries were filled with the mixture, capped at both ends and left to develop at room temperature for another 30 min, After rinsing with acetone, the capillaries were calcinated at 400 °C before use.
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We expect that the temperature inside the capillary is actually higher, perhaps significantly so, than the value read by the IR sensor in the microwave cavity. Currently, we are unable to record temperatures inside of the capillary, which would be more accurate
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We expect that the temperature inside the capillary is actually higher, perhaps significantly so, than the value read by the IR sensor in the microwave cavity. Currently, we are unable to record temperatures inside of the capillary, which would be more accurate.
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