Analyte recovery from deproteinized serum for HPLC

Journal of Liquid Chromatography and Related Technologies

Volumn 31, Issue 20, 2008, Pages 3159-3168

  Shihabi, Zak K ^a  

^a WAKE FOREST SCHOOL OF MEDICINE   (United States)

Author keywords

Acetonitrile; Capillary electrophoresis; Deproteinization; Drugs; Endogenous substances; Proteins; Recovery; Serum

Indexed keywords

ACETONITRILE; CAPILLARY ELECTROPHORESIS; METHANOL; PROTEINS; RECOVERY; SULFUR COMPOUNDS; TRICHLOROACETIC ACID; ZINC COMPOUNDS;

DEPROTEINIZATION; DRUG ANALYSIS; DRUGS; ENDOGENOUS SUBSTANCES; SAMPLE VOLUME; SERUM; SMALL MOLECULES; ZINC SULFATE;

ORGANIC SOLVENTS;

ACETONITRILE; METHANOL; TRICHLOROACETIC ACID; ZINC SULFATE;

ARTICLE; CAPILLARY ELECTROPHORESIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHOBICITY;

EID: 54349129338     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070802480156     Document Type: Article

References (16)

1. Wilson, D.W.; Helene, N.; Metz, H.N.; Graver, M.; Rao, P.S. Direct method for quantification of free malondialdehyde with high-performance capillary electrophoresis in biological samples. Clin. Chem. 1997, 43, 1982-1984.
2. Yuen, P.S.; Dunn, S.R.; Miyaji, T.; Yasuda, H.; Sharma, K.; Star, R.A. A simplified method for HPLC determination of creatinine in mouse serum. Am. J. Physiol. Renal Physiol. 2004, 286, F1116-F1119.
3. Shihabi, Z.K.; Oles, K.S. Felbamate measured in serum by two methods: HPLC and capillary electrophoresis. Clin. Chem. 1994, 40, 1904-1908.
4. Shihabi, Z.K.; Oles, K.S. Serum lamotrigine analysis by capillary electrophoresis. J. Chromatogr. B. 1996, I, 119-123.
5. Lim, J.M.; Lin, C.C. Column-switching high-performance liquid chromatographic method for determination of a new antiviral. Antimicrob. Agents Chemother. 1986, 977-979.
6. Sakuma, R.; Nishina, T.; Kitamura, M. Deproteinizing methods evaluated for determination of uric acid in Serum by reversed-phase liquid chromatography with ultraviolet detection. Clin. Chem. 1987, 33, 1427-1430.
7. Polson, C.; Sarkar, P.; Incledon, B.; Raguvaran, V.; Grant, R. Optimization of protein precipitation based upon effectiveness of protein removal and ionization effect in liquid chromatography-tandem mass spectrometry. J. Chromatogr. B. 2003, 785, 263-275.
8. Shihabi, Z.K. Sample matrix effects in capillary electrophoresis-II. Acetonitrile Deproteinization. J. Chromatogr. 1993, 652, 471-475.
9. Shihabi, Z. Transient pseudo-isotachophoresis for sample concentration in capillary electrophoresis. Electrophoresis. 2002, 23, 1612-1617.
10. Shihabi, Z.K. Stacking in capillary zone electrophoresis. J. Chromatogr. A. 2000, 902, 107-117.
11. Brkich, G.E.; Arzamastsev, A.P.; Kaz'mina, E.M.; Mikhalev, A.V. HPLC determination of pefloxacin and ciprofloxacin in blood serum. Pharm. Chem. J. 1999, 33, 219-221.
12. Hinsdale, M.E.; Lantz, P.E.; Shihabi, Z.K. Serum and tissue homocysteine analysis by HPLC. J. Liq. Chromatogr. & Rel. Technol. 1998, 21, 02715-02723.
13. Annesley, T.M.; Clayton, L. Simple extraction protocol for analysis of immunosuppressant drugs in whole blood. Clin. Chem. 2004, 50, 1845-1848.
14. Maciej, J.; Enazi, B.E.; Hassan, H.; Abdel-Jawaad, J.; Ruwaily, J.; Tufail, M. Simultaneous LC-MS-MS determination of cyclosporine A, tacrolimus, and sirolimus in whole blood as well as mycophenolic acid in plasma using common pretreatment procedure. J. Chromatogr. B. 2007, 850, 471-480.
15. Connor, E.; Sakamoto, M.; Fujikawa, K.; Law, T.; Rifai, N. Measurement of whole blood sirolimus by an HPLC assay using solid-phase extraction and UV detection. Therapeut. Drug Monitor. 2002, 24, 751-756.
16. Lam, S.; Boselli, L. HPLC of trazodone in serum after microscale protein precipitation. Biomed. Chromatogr. 2005, 1, 177-179.