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Chemistry - A European Journal

Volumn 14, Issue 12, 2008, Pages 3530-3534

Alkylzinc hydrazides: Self-assembly of hexanuclear ring systems in acetonitrile

(2) Elsegood, Mark R J b Redshaw, Carl a

a UNIVERSITY OF EAST ANGLIA (United Kingdom)

b LOUGHBOROUGH UNIVERSITY (United Kingdom)

Author keywords

Macrocycles; Selt assembly; Structurel elucidation; Zinc

Indexed keywords

ACETONITRILE; ENERGY ABSORPTION; ZINC;

MACROCYCLES; RING SYSTEMS; SELT-ASSEMBLY; STRUCTUREL ELUCIDATION;

SELF ASSEMBLY;

ACETONITRILE; ACETONITRILE DERIVATIVE; HYDRAZINE DERIVATIVE; ORGANOMETALLIC COMPOUND; ZINC;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; CRYSTALLIZATION; STEREOISOMERISM; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

ACETONITRILES; CRYSTALLIZATION; CRYSTALLOGRAPHY, X-RAY; HYDRAZINES; MODELS, MOLECULAR; MOLECULAR STRUCTURE; ORGANOMETALLIC COMPOUNDS; STEREOISOMERISM; ZINC;

EID: 53849087858 PISSN: 09476539 EISSN: 15213765 Source Type: Journal
DOI: 10.1002/chem.200800183 Document Type: Article

Times cited : (12)

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15
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- Crystal data for 3a′: C60H60F 30N18Zn6·2(C2H3N, Mr=2077.59, triclinic, space group P1̄, colourless, 0.18×0.07×0.02 mm3, a= 13.521(4, b, 13.569(4, c, 13.938(4) Å, α, 100.378(4, β=116.933(4, γ, 107.888(4)°, V=2010.1(10)Å3, T= 150(2) K, Z=1, ρcaled, 1.716gcm-3, μ, 1.884mm-1, data collected on a Bruker APEX 2 CCD diffractometer, λ=0.71073 Å, 15882 reflections measured, 7048 unique (Rint,=0.1094) which were used in all calculations. The final wR2=0.1273 (all data) and R1=0.0581 (for 3475 data with F2 2σF2, 561 parameters, largest difference map features within ±0.550 e Å-3, 16
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16
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17
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19
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- [16]

20
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21
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23
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