Development and validation of a solid-phase extraction method coupled to liquid chromatography with fluorescence detection for the determination of fluoroquinolone residues in powdered infant formulae. Application to the analysis of samples from the Spanish and Latin American market

Journal of Chromatography A

Volumn 1209, Issue 1-2, 2008, Pages 136-144

  Rodriguez, E ^a   Moreno Bondi, M C ^a   Marazuela, M D ^a  

^a UNIVERSIDAD COMPLUTENSE DE MADRID   (Spain)

Author keywords

Antibiotics; Commission Decision 2002 657 EC; Fluoroquinolones; LC FLD; Powdered infant formulae; Sample preparation

Indexed keywords

ACIDS; ANTIBIOTICS; CHROMATOGRAPHIC ANALYSIS; COLUMN CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; METHANOL; SOLVENT EXTRACTION;

COMMISSION DECISION 2002/657/EC; FLUOROQUINOLONES; LC-FLD; POWDERED INFANT FORMULAE; SAMPLE PREPARATION;

EXTRACTION;

CIPROFLOXACIN; DANOFLOXACIN; ENROFLOXACIN; METHANOL; NORDIFLOXACIN; TRICHLOROACETIC ACID;

ARTICLE; ARTIFICIAL MILK; DRUG ISOLATION; DRUG STRUCTURE; FLUORESCENCE ANALYSIS; LIQUID CHROMATOGRAPHY; MARKET; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; SOUTH AND CENTRAL AMERICA; VALIDATION STUDY;

CHROMATOGRAPHY, LIQUID; CIPROFLOXACIN; FLUOROQUINOLONES; HUMANS; INFANT; INFANT FORMULA; LATIN AMERICA; MOLECULAR STRUCTURE; REPRODUCIBILITY OF RESULTS; SOLID PHASE EXTRACTION; SPAIN; SPECTROMETRY, FLUORESCENCE;

BOVINAE;

EID: 53749091511     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2008.09.031     Document Type: Article

References (25)

1. WHO global strategy for containment of antimicrobial resistance, Executive summary 2001, World Health Organization (WHO), Geneva.
2. Meeting on Antimicrobial Resistance, Brussels, January 17, 2008, http://ec.europa.eu/food/resources/events_en.htm.
3. Duffy G., Lynch O.A., and Cagney C. Meat Sci. 78 (2008) 34
4. Commission Regulation 1353/2007/EC of 20 November, amending Council Regulation 2377/90/EC laying down a Community procedure for the establishment of maximum residue limits of veterinary medicinal products in foodstuffs of animal origin, Off. J. Eur. Union L, 303, 2007.
5. Lupin J.R. Critic. Rev. Food Sci. Nutr. 42 (2002) 403
6. Joint FAO/WHO Food Standards Programme Codex Alimentarius Commission, Report of the 17th session of the Codex Committee on residues of veterinary drugs in foods, Breckenridge, CO, September 3-7, 2007.
7. Commission Directive 2006/141/EC of 22 December 2006 on infant formulae and follow-on formulae amending Directive 1999/21/EC, Off. J. Eur. Union L, 401, 2006.
8. Commission Regulation 856/2005/EC of 6 June, amending Council Regulation 466/2001/EC, as regards Fusarium toxins, Off. J. Eur. Union L, 143, 2005.
9. Andreu V., Blasco C., and Picó Y. Trends Anal. Chem. 26 (2007) 534
10. Cinquina A.L., Roberti P., Giannetti L., Longo F., Draisci R., Fagiolo A., and Brizioli N.R. J. Chromatogr. A 987 (2003) 221
11. Marazuela M.D., and Moreno-Bondi M.C. J. Cromatogr. A 1034 (2004) 25
12. Idowu O.R., and Peggins J.O. J. Pharm. Biomed. Anal. 35 (2004) 143
13. Ho C., Sin D.W.M., Tang H.P.O., Cheng L.P.K., and Siu S.M.P. J. Chromatogr. A 1061 (2004) 123
14. Van Hoof N., De Wash K., Okerman L., Reybroeck W., Poelmans S., Noppe H., and De Brabander H. Anal. Chim. Acta 529 (2005) 265
15. Yang G., Lin B., Zeng Z., Cheng Z., and Huang X. J. AOAC Int. 88 (2005) 1688
16. Christodoulou E.A., and Samanidou V.F. J. Sep. Sci. 30 (2007) 2429
17. Hermo M.P., Nemutlu E., Kir S., Barrón D., and Barbosa J. Anal. Chim. Acta 613 (2008) 98
18. Bogialli S., D'Ascenzo G., di Corcia A., Laganà A., and Nicolardi S. Food Chem. 108 (2008) 354
19. Koletzko B., Baker S., Cleghorn G., Neto U.F., Gopalan S., Hernell O., Hock Q.S., Jirapinyo P., Lonnerdal B., Pencharz P., Pzyrembel H., Ramirez J., Shamir R., Turck D., Yamashiro Y., and Zong-Yi D. J. Pediatr. Gastroenterol. Nutr. 41 (2005) 584
20. Commission Decision 2002/657/EC of 12 August implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of the results, Off. J. Eur. Union L, 221, 2002.
21. Council Directive 96/23/EC of 29 April on measures to monitor certain substances and residues thereof in live animals and animal products, Off. J. Eur. Union L, 125, 1996.
22. Volmer D.A., Mansoori B., and Locke S.J. Anal. Chem. 69 (1997) 4143
23. Fletouris D.J. In: Picó Y. (Ed). Food Toxicants Analysis, Techniques, Strategies and Developments (2007), Elsevier, Amsterdam 337
24. Zeleny R., Ulberth F., Gowik P., Polzer J., van Ginkel L.A., and Emons H. Trends Anal. Chem. 25 (2006) 927
25. Guidelines for the implementation of Decision 2002/657/EC, European Commission SANCO/2004/2726rev1, Chapter 2: Performance criteria and other requirements for analytical methods, European Union, Brussels.