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detailed conditions are described in the Supporting Information
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21
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53549112440
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6 salt) and the ESR spectra of 2 recorded at several microwave powers are shown in Figures S1 and S2, respectively, of the Supporting Information.
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6 salt) and the ESR spectra of 2 recorded at several microwave powers are shown in Figures S1 and S2, respectively, of the Supporting Information.
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22
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53549094645
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2] is shown in Figure S3 of the Supporting Information.
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2] is shown in Figure S3 of the Supporting Information.
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23
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53549085945
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The quality of the crystals was improved by adding 1-adamantanol as a template
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The quality of the crystals was improved by adding 1-adamantanol as a template.
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24
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53549132225
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The ESR spectra of 2 recorded at different concentrations and temperatures are shown in Figures S4 and S5 of the Supporting Information.
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The ESR spectra of 2 recorded at different concentrations and temperatures are shown in Figures S4 and S5 of the Supporting Information.
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25
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0003431029
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2nd ed, Wiley-Intersciene
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Weil, J.A.1
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26
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0035805361
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The nitrosyl radicals 3 and 4 that were used as guests were prepared by the improved Ullman's procedure described in the following reference: C. Hirel, K. E. Vostrikova, J. Pecaut, V. I. Ovcharenko, P. Rey, Chem. Eur. J. 2001, 7, 2007-2014.
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The nitrosyl radicals 3 and 4 that were used as guests were prepared by the improved Ullman's procedure described in the following reference: C. Hirel, K. E. Vostrikova, J. Pecaut, V. I. Ovcharenko, P. Rey, Chem. Eur. J. 2001, 7, 2007-2014.
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53549123244
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2·3: Elemental analysis calcd for C128H 104N52O36Pd6·C 21H21N2O2·21H2O: C 41.65, H 3.92, N 17.60; found: C 41.75, H 4.04, N 17.38. 2·(4) 2: Elemental analysis calcd for C128H 104N52O36Pd6·2C 17H19N2O2·22H2O: C 42.78, H 4.12, N 17.25; found: C 42.82, H 4.10, N 17.11. The extraction experiments are described in Section 7 of the Supporting Information
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2O: C 42.78, H 4.12, N 17.25; found: C 42.82, H 4.10, N 17.11. The extraction experiments are described in Section 7 of the Supporting Information.
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53549132498
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The χT versus T plots of 2 and 2·3 are shown in Figure S6 of the Supporting Information.
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The χT versus T plots of 2 and 2·3 are shown in Figure S6 of the Supporting Information.
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The enclathration of neutral molecules is described in the Supporting Information
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The enclathration of neutral molecules is described in the Supporting Information.
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