Coherence selection in double CP MAS NMR spectroscopy

Journal of Magnetic Resonance

Volumn 195, Issue 1, 2008, Pages 116-120

  Yang, Jen Hsien ^a   Chou, Fang Chieh ^b   Tzou, Der Lii M ^a,c  

^a INSTITUTE OF CHEMISTRY   (Taiwan)

^b NATIONAL TAIWAN UNIVERSITY   (Taiwan)

^c NATIONAL CHIAYI UNIVERSITY   (Taiwan)

Author keywords

Coherent transfer; Double cross polarization; Magic angle spinning; Solid state NMR; Spectral editing

Indexed keywords

NUCLEAR MAGNETIC RESONANCE;

COHERENT TRANSFER; DOUBLE CROSS-POLARIZATION; MAGIC-ANGLE SPINNING; SOLID-STATE NMR; SPECTRAL EDITING;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ALGORITHM; ARTICLE; CHEMICAL MODEL; COMPUTER SIMULATION; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SPIN LABELING;

ALGORITHMS; COMPUTER SIMULATION; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, CHEMICAL; SPIN LABELS;

EID: 53549113035     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2008.08.006     Document Type: Article

References (18)

1. Schaefer J., Mckay R.A., and Stejskal E.O. Double-cross-polarization NMR of solids. J. Magn. Reson. 34 (1979) 443-447
2. Fujiwara T., Sugase K., Kainosho M., Ono A., Ono A., and Akutsu H. C-13-C-13 and C-13-N-15 dipolar correlation NMR of uniformly labeled organic-solids for the complete assignment of their C-13 and N-15 signals-an application to adenosine. J. Am. Chem. Soc. 117 (1995) 11351-11352
3. Vaneck E.R.H., and Veeman W.S. Solid-state 2D-heteronuclear Al-27-P-31 correlation NMR-spectroscopy of aluminophosphate Vpi-5. J. Am. Chem. Soc. 115 (1993) 1168-1169
4. Ramanathan K.V., and Opella S.J. High-resolution solid-state C-13-N-14 and C-13-N-15 heteronuclear correlation spectroscopy. J. Magn. Reson. 86 (1990) 227-235
5. Baldus M., Petkova A.T., Herzfeld J., and Griffin R.G. Cross polarization in the tilted frame: assignment and spectral simplification in heteronuclear spin systems. Mol. Phys. 95 (1998) 1197-1207
6. Tzou D.L.M. A solid-state NMR application of the anoineric effect in carbohydrates: galactosamine, glucosamine, and N-acetyl-glucosamine. Solid State Nucl. Magn. Reson. 27 (2005) 209-214
7. Baldus M., Geurts D.G., Hediger S., and Meier B.H. Efficient N-15-C-13 polarization transfer by adiabatic-passage Hartmann-Hahn cross polarization. J. Magn. Reson. A 118 (1996) 140-144
8. Hediger S., Meier B.H., Kurur N.D., Bodenhausen G., and Ernst R.R. NMR cross-polarization by adiabatic passage through the Hartmann-Hahn condition (Aphh). Chem. Phys. Lett. 223 (1994) 283-288
9. Hediger S., Meier B.H., and Ernst R.R. Adiabatic passage Hartmann-Hahn cross-polarization in NMR under magic-angle sample-spinning. Chem. Phys. Lett. 240 (1995) 449-456
10. Zhang S.M., Czekaj C.L., and Ford W.T. Enhancement of polarization transfer under high-speed MAS using a quasi-adiabatic cross-polarization sequence. J. Magn. Reson. A 111 (1994) 87-92
11. Zhang S.M. Quasi-adiabatic polarization transfer in solid-state NMR. J. Magn. Reson. A 110 (1994) 73-76
12. Meier B.H. Cross polarization under fast magic angle spinning-thermodynamical considerations. Chem. Phys. Lett. 188 (1992) 201-207
13. Gullion T., and Schaefer J. Rotational-echo double-resonance NMR. J. Magn. Reson. 81 (1989) 196-200
14. Mehring M. Principles of High Resolution NMR in Solids. second ed. (1983), Springer, Berlin
15. Takegoshi K., Nomura K., and Terao T. Selective homonuclear polarization transfer in the tilted rotating frame under magic angle spinning in solids. J. Magn. Reson. 127 (1997) 206-216
16. Costa P.R., Sun B.Q., and Griffin R.G. Rotational resonance tickling: accurate internuclear distance measurement in solids. J. Am. Chem. Soc. 119 (1997) 10821-10830
17. Hartmann S.R., and Hahn E.L. Nuclear double resonance in the rotating frame. Phys. Rev. 128 (1962) 2043-2053
18. Bennett A.E., Rienstra C.M., Auger M., Lakshmi K.V., and Griffin R.G. Heteronuclear decoupling in rotating solids. J. Chem. Phys. 103 (1995) 6951-6954