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The preparation of 2a
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-1): 3401, 1617, 1504, 1458, 1423, 1354, 1333, 1289, 1253, 1203, 1132, 894, 745, 723, 626, 534, 479, 427.
-
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48
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53149136677
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The compound 2b
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-1): 3446, 3081, 3031, 1613, 1495, 1452, 1443, 1377, 1367, 1333, 1286, 1266, 1203, 1188, 974, 888, 777, 766, 739, 732, 696, 475, 425.
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37049097168
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65
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53149145135
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-
note
-
2O (0.043 g, 0.254 mmol) in methylene chloride (30 mL) was added to the above residue in methylene chloride (30 mL), and the reaction mixture was stirred at room temperature for 23 h. The reaction solvent was removed and the resulting solid was washed with hexane (30 mL) and dried in vacuo (0.090 g, 48.0%).
-
-
-
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67
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53149093696
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note
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2).
-
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68
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37049078495
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