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Crystal data and structure refinement for 1: black plate (0.25 x 0.15 x 0.05 mm3, triclinic, space group P1, a, 1720.1(1, b, 1756.2(1, c, 2434.3(2) pm, α, 110.071(1, β, 91.569(1, γ, 92.670(1)°, V, 6893(1) × 10 6 pm3, ρcalcd, 1.931 g cm-3, Z, 2, μ-(MoKα, 7.56 mm-1, λ, 71.073 pm, Bruker AXS Smart APEX diffractometer, graphite monochromator, ω scan, semiempirical absorption correction (SADABS; G. M. Sheldrick, 2.10 ed, Bruker AXS, Madison, WI, USA, 2003, structure solution and refinement with SHELXTL (G. M. Sheldrick, Version 6.10 ed, Bruker AXS, Madison, WI, USA, 2000, T, 100 K, 59471 measured reflections, 30380 symmetry-independent reflections 2θmax, 55.00°, 1822 refined parameters, R1, 0.0381, wR2, 0
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