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52949101822
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note
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-1): 3422(vs/b), 3247(m/b), 3063(w), 1626(s), 1585(m), 1520(s), 1428(vs), 1346(w), 1306(w), 1193(s), 1125(vs), 1032(vs), 970(vs), 946(vs), 908(w), 871(m), 848(vs), 776(m), 737(m), 723(vs), 648(w), 618(w), 595(m), 509(w), 431(m).
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40
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52949139168
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note
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2 = 0.1488, GOF = 1.049 for all 10059 data. The structure was solved by direct methods and refined by full-matrix least-squares methods using SHELXS97 and SHELXL97 programs [14], respectively. Non-hydrogen atoms were determined with successive difference Fourier syntheses and refined anisotropically. The O13 atom of the one sulfato groups was found disordered. H atoms attached on C were placed in the calculated positions, whereas the H atoms of water molecule were found from the Fourier map and treated as riding atoms.
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41
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52949152516
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G.M. Sheldrick, SHELXS97, Program for the solution of crystal structures, University of Göttingen, Germany, 1997; G.M. Sheldrick, SHELXL97, Program for the Refinement of Crystal Structures, University of Göttingen, Germany, 1997.
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G.M. Sheldrick, SHELXS97, Program for the solution of crystal structures, University of Göttingen, Germany, 1997; G.M. Sheldrick, SHELXL97, Program for the Refinement of Crystal Structures, University of Göttingen, Germany, 1997.
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