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The crystal data of 4 were collected on a Bruker X8Apex diffractometer with a CCD area detector and multilayer mirror-monochromated Mo Kα radiation. The structure was solved using direct methods, refined with the SHELX software package (G. Sheldrick, University of Göttingen, 1997) and expanded using Fourier techniques. All non-hydrogen atoms were refined anisotropically. Hydrogen atoms were assigned idealized positions and were included in structure factor calculations. Crystal data for 4: C 92H54B3F48FeN3, Mr, 2201.66, orange block, 0.210 x 0.205 x 0.200, triclinic space group P1, a, 13.1283(4) Å, b, 13.4927(4) Å, c, 26.7028(8) Å, α, 86.4180(10)°, β, 84.8160(10)°, γ, 78.3220(10)°, V, 4608.4(2) Å3, Z, 2, ρcalcd, 1.587 g cm -3, μ, 0.310 mm
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