메뉴 건너뛰기




Volumn 47, Issue 17, 2008, Pages 7456-7458

Synthesis and structure of a ferrocenylboron dication

Author keywords

[No Author keywords available]

Indexed keywords


EID: 51849112767     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic800876p     Document Type: Article
Times cited : (29)

References (32)
  • 17
    • 51849163167 scopus 로고    scopus 로고
    • The crystal data of 4 were collected on a Bruker X8Apex diffractometer with a CCD area detector and multilayer mirror-monochromated Mo Kα radiation. The structure was solved using direct methods, refined with the SHELX software package (G. Sheldrick, University of Göttingen, 1997) and expanded using Fourier techniques. All non-hydrogen atoms were refined anisotropically. Hydrogen atoms were assigned idealized positions and were included in structure factor calculations. Crystal data for 4: C 92H54B3F48FeN3, Mr, 2201.66, orange block, 0.210 x 0.205 x 0.200, triclinic space group P1, a, 13.1283(4) Å, b, 13.4927(4) Å, c, 26.7028(8) Å, α, 86.4180(10)°, β, 84.8160(10)°, γ, 78.3220(10)°, V, 4608.4(2) Å3, Z, 2, ρcalcd, 1.587 g cm -3, μ, 0.310 mm
    • -1, F(000) = 2200, T = 100(2) K, R1 = 0.0611, wR2 = 0.1319, 17 959 independent reflections [2θ ≤ 52.04°] and 1385 parameters. Crystallographic data have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication CCDC 687804. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.