Ultrasonic extraction of veterinary antibiotics from soils and pig slurry with SPE clean-up and LC-UV and fluorescence detection

Talanta

Volumn 64, Issue 4, 2004, Pages 1058-1064

  Blackwell, Paul A ^a,c   Holten Lützhøft, Hans Christian ^b   Ma, Hai Ping ^b   Halling Sørensen, Bent ^b   Boxall, Alistair B A ^a   Kay, Paul ^a  

^a Cranfield Centre for EcoChemistry   (United Kingdom)

^b UNIVERSITY OF COPENHAGEN   (Denmark)

^c ENVIRONMENT AGENCY   (United Kingdom)

Author keywords

Pig slurry; Soils; Ultrasonic extraction; Veterinary antibiotics

Indexed keywords

ANTIBIOTICS; EXTRACTION; FLUORESCENCE; POLYMERS; SLURRIES; ULTRASONICS; VETERINARY MEDICINE;

ANION EXCHANGE; OXYTETRACYCLINE (OTC); SOLID PHASE EXTRACTION (SPE); TYLOSIN (TYL);

SOILS;

ANTIBIOTIC AGENT; EDETIC ACID; MACROLIDE; METHANOL; ORGANIC MATTER; OXYTETRACYCLINE; POLYMER; SULFACHLORPYRIDAZINE; SULFADIMIDINE; SULFATHIAZOLE; SULFONAMIDE; TYLOSIN;

ANION EXCHANGE; ARTICLE; CLAY; DRUG ISOLATION; FLUORESCENCE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; PH; SOIL; SOLID PHASE EXTRACTION; SWINE; ULTRAVIOLET SPECTROSCOPY; VORTEX MOTION;

EID: 5144223504     PISSN: 00399140     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.talanta.2004.05.006     Document Type: Article

References (31)

1. Halling-Sørensen B., Nors Nielsen S., Lanzky P.F., Ingerslev F., Holten Lützhøft H.-C., Jørgensen S.E. Chemosphere. 36:1998;357
2. Hamscher G., Sczesny S., Höper H., Nau H. Anal. Chem. 74:2002;1509
3. Golet E.M., Strehler A., Alder A.C., Giger W. Anal. Chem. 74:2002;5455
4. Marengo J.R., Kok R.A., O'Brien K., Velagaleti R.R., Stamm J.M. Environ. Toxicol. Chem. 16:1997;462
5. Weerasinghe C.A., Towner D. Environ. Toxicol. Chem. 16:1997;1873
6. Westergaard K., Müller A.K., Christensen S., Bloem J., Sørensen S.J. Soil Biol. Biochem. 33:2001;2061
7. Bewick M.W.M. Plant Soil. 51:1979;363
8. L.H. Hansen, F. Aarestrup, S.J. Sørensen, Vet. Microbiol. 87 (2002) 51.
9. Kühne M., Ihnen D., Möller G., Agthe O. J. Vet. Med. A. 47:2000;379
10. Pfeifer T., Tuerk J., Bester K., Spiteller M. Rapid Commun. Mass Spectrom. 16:2002;663
11. Haller M.Y., Müller S.R., McArdell C.S., Alder A.C., Suter M.J.-F. J. Chromatogr. A. 952:2002;111
12. Boxall A.B.A., Fogg L.A., Kay P., Blackwell P.A., Pemberton E.J., Croxford A. Toxicol. Lett. 142:2003;207
13. Stephens C.R., Murai K., Brunning K.J., Woodward R.B. J. Am. Chem. Soc. 78:1956;4155
14. Schumacher G.E., Linn E.E. J. Pharm. Sci. 67:1978;1717
15. Novartis. Sulfachloropyridazine safety data sheet, release date 18 October 1999.
16. Tolls J. Environ. Sci. Technol. 35:2001;3397
17. J.M. Hodgson (Ed.), Soil survey field handbook: describing and sampling soil profiles, Soil Survey Technical Monograph No. 5, Harpenden, 1976.
18. Spaepen K.R.I., Van Leemput L.J.J., Wislocki P.G., Verschueren C. Environ. Toxicol. Chem. 16:1997;1977
19. Thompson M., Ellison S.L.R., Wood R. Pure Appl. Chem. 74:2002;835
20. Dean J.R., Xiong G. Trends Anal. Chem. 19:2000;553
21. Miège C., Dugay J., Hennion M.-C. J. Chromatogr. A. 823:1998;219
22. Hawthorne S.B., Grabanski C.B., Martin E., Miller D.J. J. Chromatogr. A. 892:2000;421
23. Saim N., Dean J.R., Abdullah M.P., Zakaria Z. J. Chromatogr. A. 791:1997;361
24. Sun F., Littlejohn D., Gibson M.D. Anal. Chim. Acta. 364:1998;1
25. Babié S., Petrovié M., Kaštelan-Macan M. J. Chromatogr. A. 823:1998;3
26. Boxall A.B.A., Blackwell P., Cavallo R., Kay P., Tolls J. Toxicol. Lett. 131:2002;19
27. Rabølle M., Spliid N.H. Chemosphere. 40:2000;715
28. Loke M.-L., Tjørnelund J., Halling-Sørensen B. Chemosphere. 48:2002;351
29. Oka H., Ito Y., Matsumoto H. J. Chromatogr. A. 882:2000;109
30. Tsai C.-E., Kondo F. J. AOAC Int. 78:1995;674
31. Takeda N., Akiyama Y. J. Chromatogr. 558:1991;175