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Preparation of 6-(2′-hydroxybenzoyl)-5-methyl-7-phenyl-pyrazolo[1,5-a]pyrimidines 5a-h: A mixture of equimolar amounts of 5-amino-3-R-1H-pyrazole 1 (10 mmol) and 3-benzoyl-2-methyl-4H-chromen-4-one 4 (2.64 g, 10 mmol) was heated in an oil-bath at 180 °C for 2 min (Method A) or was placed in an air open Pyrex-erlenmeyer flask, and the system was irradiated in a multimode microwave oven during 2 min (at 600 W) (Method B).
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2: m/z = 419.1634; found: 419.1639.
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