-
6
-
-
33751154718
-
-
Yang L.-W., Liu S., Wong E., Rettig S.J., and Orvig C. Inorg. Chem. 34 (1995) 2164
-
(1995)
Inorg. Chem.
, vol.34
, pp. 2164
-
-
Yang, L.-W.1
Liu, S.2
Wong, E.3
Rettig, S.J.4
Orvig, C.5
-
7
-
-
50249107685
-
-
note
-
-1 on a BRUKER Vector22 spectrometer.
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-
-
-
8
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-
50249157107
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-
note
-
2) / 3), Difference Fourier residues [-0.5, +0.71]e-/Å3. The crystal structure measurement was made on an X8 Bruker diffractometer (Apex 2 area detector) equipped with a graphite monochromated Mo Kα radiation. The Intensities were integrated from the collected frames and corrected for background, Lorentz and polarization effects, using SAINT [Bruker Analytical X-ray system, ''SAINT+, Version 7.12'', Madison, USA, 2004] and for crystal/detector area absorption from the SADABS software [G.M. Scheldrick, SADABS, Bruker-Siemens Area Detector Absorption and Other Correction, Version 2006/1, Göttingen Germany, 2006]. The lattice parameters were refined from the complete data set. The structure was solved primarily by direct method and second by Fourier difference techniques [G.M. Sheldrick, SHELXS 97, Program for the Solution of Crystal Structures, University of Göttingen, Germany, 1997]. The structure refinement was performed with the SHELXL-97 software [G.M. Sheldrick, SHELXL 97, Program for the Refinement of Crystal Structures, University of Göttingen, Germany, 1997] by the full-matrix least-squares method. All the non-hydrogen atoms positions were anisotropically refined. The hydrogen atoms were determined on Fourier difference map and were isotropically refined. The H atoms of the water molecule were not found because of a great isotropic displacement of the O2h atom.
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-
-
-
10
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-
4744366734
-
-
Schuetz S.A., Silvernail C.M., Incarvito C.D., Rheingold A.L., Clark J.L., Day V.W., and Belot J.A. Inorg. Chem. 43 (2004) 6203
-
(2004)
Inorg. Chem.
, vol.43
, pp. 6203
-
-
Schuetz, S.A.1
Silvernail, C.M.2
Incarvito, C.D.3
Rheingold, A.L.4
Clark, J.L.5
Day, V.W.6
Belot, J.A.7
-
11
-
-
2942629657
-
-
Kanesato M., Mizukami S., Houjou H., Tokuhisa H., Koyama E., and Nagawa Y. J. Alloys Compds. 374 (2004) 307
-
(2004)
J. Alloys Compds.
, vol.374
, pp. 307
-
-
Kanesato, M.1
Mizukami, S.2
Houjou, H.3
Tokuhisa, H.4
Koyama, E.5
Nagawa, Y.6
-
14
-
-
0038412630
-
-
Kano S., Nakano H., Lojima M., Baba N., and Nakajima K. Inorg. Chem. Acta 349 (2003) 6
-
(2003)
Inorg. Chem. Acta
, vol.349
, pp. 6
-
-
Kano, S.1
Nakano, H.2
Lojima, M.3
Baba, N.4
Nakajima, K.5
-
15
-
-
33748503714
-
-
Howell .R.C., Spence K.V.N., Kahwa I.A., and Williams D.J. J. Chem. Soc., Dalton Trans. (1998) 2727
-
(1998)
J. Chem. Soc., Dalton Trans.
, pp. 2727
-
-
Howell, .R.C.1
Spence, K.V.N.2
Kahwa, I.A.3
Williams, D.J.4
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