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Volumn 902, Issue , 2005, Pages 259-302

(1R)-4-amino-1,2,4-triazolium salts: New families of ionic liquids

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EID: 49249092608     PISSN: 00976156     EISSN: None     Source Type: Book Series    
DOI: 10.1021/bk-2005-0902.ch020     Document Type: Conference Paper
Times cited : (22)

References (108)
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    • X-ray Crystallography. The single crystal X-ray diffraction data were collected on a Bruker 3-circle platform diffractometer equipped with a SMART CCD (charge coupled device) detector with the χ-axis fixed at 54.74° and using MoKα radiation (α, 0.71073 Å) from a fine-focus tube. This diffractometer was equipped with KryoFlex apparatus for low temperature data collection using controlled liquid nitrogen boil off. The goniometer head, equipped with a nylon Cryoloop with a magnetic base, was then used to mount the crystals using PFPE (perfluoropolyether) oil. Cell constants were determined from 90 ten-second frames. A complete hemisphere of data was scanned on omega (0.3°) with a run time often-second per frame at a detector resolution of 512 × 512 pixels using me SMART software.1 A total of 1271 frames were collected in three sets and final sets of 50 frames, identical to the first 50 frames, were also collected to determine any
    • 6 All non-hydrogen atoms were refined anisotropically. For the anisotropic displacement parameters, me U(eq) is defined as one third of the trace of the orthogonalized Uij tensor. The hydrogen atoms were located either from difference electron density maps or generated at calculated positions . 1. SMART V 4.045 Software for the CCD Detector System, Bruker AXS, Madison, WI, 1999. 2. SAINT V 4.035 Software for the CCD Detector System Bruker AXS, Madison, WI , 1999. 3. SADABS, Program for absorption correction for area detectors Version 2.01, Bruker AXS, Madison, WI, 2000. 4. Sheldrick, G. M. SHELXS-90, Program for the Solution of Crystal Structure University of Göttingen, Germany, 1990. 5. Sheldrick, G. M. SHELXL-97, Program for the Refinement of Crystal Structure University of Göttingen, Germany, 1997. 6. SHELXTL 5.10 for Windows NT, Program library for Structure Solution and Molecular Graphics Bruker AXS, Madison, WI, 2000.
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.