Quantitative time- and frequency-domain analysis of the two-pulse COSY revamped by asymmetric Z -gradient echo detection NMR experiment: Theoretical and experimental aspects, time-zero data truncation artifacts, and radiation damping

Journal of Chemical Physics

Volumn 129, Issue 4, 2008, Pages

  Kirsch, Stefan ^a   Hull, William E ^a  

^a GERMAN CANCER RESEARCH CENTER DKFZ   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

COHERENT LIGHT; DAMPING; ERROR ANALYSIS; EXPERIMENTS; FERROMAGNETISM; FOURIER ANALYSIS; FOURIER TRANSFORMS; FREQUENCY DOMAIN ANALYSIS; GRADIENT METHODS; INTEGRAL EQUATIONS; LEAST SQUARES APPROXIMATIONS; NONLINEAR EQUATIONS; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RADIATION; SET THEORY;

ANALYTICAL FUNCTIONS; AND RECOVERY; BINOMIAL COEFFICIENTS; BLOCH EQUATIONS; DATA POINTS; DATA SETS; DATA TRUNCATION; DEMAGNETIZING FIELDS; EVOLUTION TIME; EXPERIMENTAL ASPECTS; EXPONENTIAL DECAYS; FIRST-ORDER APPROXIMATIONS; FIRST-ORDER MODELS; FOURIER; FOURIER TRANSFORMATIONS; FREE VARIABLES; GRADIENT-ECHO; INDUCTION DECAY; INTER-MOLECULAR MULTIPLE-QUANTUM COHERENCES; LEAST-SQUARES FITS; LINE SHAPES; LORENTZIANS; PHASE CYCLING; RADIATION DAMPING; REFERENCE VALUES; SAMPLE TUBE; SCALING FUNCTIONS; SIGNAL AMPLITUDES; SINGLE-QUANTUM COHERENCE; TIME-DOMAIN FITTING; TRANSVERSE MAGNETIZATION; WATER SAMPLES;

TIME DOMAIN ANALYSIS;

NICKEL; WATER;

ARTICLE; ARTIFACT; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; QUANTUM THEORY; RADIATION; TIME;

ARTIFACTS; MAGNETIC RESONANCE SPECTROSCOPY; NICKEL; QUANTUM THEORY; RADIATION; TIME FACTORS; WATER;

EID: 49149117466     PISSN: 00219606     EISSN: None     Source Type: Journal    
DOI: 10.1063/1.2951993     Document Type: Article

References (51)

1. E. L. Hahn, Phys. Rev. 0031-899X 80, 580 (1950).
2. M. H. Levitt, Concepts Magn. Reson. 1043-7347 10.1002/(SICI)1099- 0534(1996)8:2<77::AID-CMR1>3.0.CO;2-L 8, 77 (1996).
3. H. T. Edzes, J. Magn. Reson. (1969-1992) 0022-2364 10.1016/0022-2364(90) 90261-7 86, 293 (1990).
4. G. Deville, M. Bernier, and J. M. Delrieux, Phys. Rev. B 0163-1829 10.1103/PhysRevB.19.5666 19, 5666 (1979).
5. D. Einzel, G. Eska, and Y. Hirayoshi, Phys. Rev. Lett. 0031-9007 10.1103/PhysRevLett.53.2312 53, 2312 (1984).
6. R. Bowtell, R. M. Bowley, and P. Glover, J. Magn. Reson. (1969-1992) 0022-2364 10.1016/0022-2364(90)90297-M 88, 643 (1990).
7. R. P. O. Jones, G. A. Morris, and J. C. Waterton, J. Magn. Reson. (1969-1992) 0022-2364 10.1016/0022-2364(92)90114-M 98, 115 (1992).
8. A. S. Bedford, R. Bowtell, and R. M. Bowley, J. Magn. Reson. (1969-1992) 0022-2364 10.1016/0022-2364(91)90080-D 93, 516 (1991).
9. I. Ardelean, R. Kimmich, S. Stapf, and D. E. Demco, J. Magn. Reson. 1090-7807 10.1006/jmre.1997.1197 127, 217 (1997).
10. I. Ardelean and R. Kimmich, J. Magn. Reson. 1090-7807 10.1006/jmre.1999.1975 143, 101 (2000).
11. I. Ardelean, B. Buhai, and R. Kimmich, Appl. Magn. Reson. 26, 307 (2004). 0937-9347
12. Q. He, W. Richter, S. Vathyam, and W. S. Warren, J. Chem. Phys. 0021-9606 10.1063/1.464770 98, 6779 (1993).
13. S. Lee, W. Richter, S. Vathyam, and W. S. Warren, J. Chem. Phys. 0021-9606 10.1063/1.471968 105, 874 (1996).
14. W. S. Warren, W. Richter, A. H. Andreotti, and B. T. Farmer, Science 0036-8075 10.1126/science.8266096 262, 2005 (1993).
15. S. Vathyam, S. Lee, and W. S. Warren, Science 0036-8075 10.1126/science.272.5258.92 272, 92 (1996).
16. P. Robyr and R. Bowtell, J. Chem. Phys. 0021-9606 10.1063/1.473388 106, 467 (1997).
17. W. S. Warren, S. Ahn, M. Mescher, M. Garwood, K. Ugurbil, W. Richter, R. R. Rizi, J. Hopkins, and J. S. Leigh, Science 0036-8075 10.1126/science.281. 5374.247 281, 247 (1998).
18. J. Zhong, Z. Chen, and E. Kwok, Magn. Reson. Med. 0740-3194 10.1002/(SICI)1522-2594(200003)43:3<335::AID-MRM3>3.0.CO;2-1 43, 335 (2000).
19. J. Zhong, Z. Chen, and E. Kwok, J. Magn. Reson Imaging 12, 311 (2000). 1053-1807
20. W. Richter, M. Richter, W. S. Warren, H. Merkle, P. Andersen, G. Adriany, and K. Ugurbil, Magn. Reson. Imaging 0730-725X 10.1016/S0730-725X(00)00133-8 18, 489 (2000).
21. S. Capuani, F. Cruzi, F. M. Alessandri, B. Maraviglia, and A. Bifone, Magn. Reson. Med. 0740-3194 10.1002/mrm.1246 46, 683 (2001).
22. S. Gutteridge, C. Ramanathan, and R. Bowtell, Magn. Reson. Med. 0740-3194 10.1002/mrm.10142 47, 871 (2002).
23. F. Fasano, S. Capuani, G. E. Hagberg, T. Branca, I. Indovina, A. Castriota-Scanderbeg, and B. Maraviglia, Magn. Reson. Imaging 21, 1151 (2003). 0730-725X
24. X. P. Tang, C. L. Chin, L. S. Bouchard, F. W. Wehrli, and W. S. Warren, Phys. Lett. A 0375-9601 10.1016/j.physleta.2004.04.017 326, 114 (2004).
25. S. Kirsch and P. Bachert, J. Magn. Reson. 1090-7807 10.1016/j.jmr.2006. 10.011 185, 183 (2007).
26. W. Barros, Jr., J. C. Gore, and D. F. Gochberg, J. Magn. Reson. 1090-7807 10.1016/j.jmr.2005.09.013 178, 166 (2006).
27. I. Ardelean, E. Kossel, and R. Kimmich, J. Chem. Phys. 0021-9606 10.1063/1.1365111 114, 8520 (2001).
28. C. Ramanathan and R. Bowtell, J. Chem. Phys. 0021-9606 10.1063/1.1375026 114, 10854 (2001).
29. J. P. Marques, S. Grant, S. Blackband, and R. W. Bowtell, J. Chem. Phys. 0021-9606 10.1063/1.2085169 123, 164311 (2005).
30. B. Zheng, Z. Chen, S. Cai, J. Zhong, and C. Ye, J. Chem. Phys. 0021-9606 10.1063/1.2001652 123, 074317 (2005).
31. R. Kimmich and I. Ardelean, J. Chem. Phys. 0021-9606 10.1063/1.478261 110, 3708 (1999).
32. I. Ardelean and R. Kimmich, J. Chem. Phys. 0021-9606 10.1063/1.481123 112, 5275 (2000).
33. J. Jeener, J. Chem. Phys. 0021-9606 10.1063/1.481063 112, 5091 (2000).
34. S. Ahn and W. S. Warren, Chem. Phys. Lett. 0009-2614 10.1016/S0009- 2614(98)00532-6 291, 121 (1998).
35. E. D. Minot, P. T. Callaghan, and N. Kaplan, J. Magn. Reson. 1090-7807 10.1006/jmre.1999.1793 140, 200 (1999).
36. G. D. Charles-Edwards, G. S. Payne, M. O. Leach, and A. Bifone, J. Magn. Reson. 1090-7807 10.1016/j.jmr.2003.10.017 166, 215 (2004).
37. G. J. Bowden, T. Heseltine, and M. J. Prandolini, Chem. Phys. Lett. 0009-2614 10.1016/0009-2614(94)01502-M 233, 639 (1995).
38. J. Jeener, in Encyclopedia of Nuclear Magnetic Resonance, Advances in NMR, Vol. 9, edited by, D. M. Grant, and, R. K. Harris, (Wiley, Chichester, 2002), pp. 642-679.
39. S. Y. Huang, Y. -Y. Lin, N. Lisitza, and W. S. Warren, J. Chem. Phys. 0021-9606 10.1063/1.1467333 116, 10325 (2002).
40. S. Y. Huang, J. D. Walls, Y. Wang, W. S. Warren, and, Y. -Y. Lin, J. Chem. Phys. 0021-9606 10.1063/1.1802492 121, 6105 (2004).
41. S. Datta, S. Y. Huang, and, Y. -Y. Lin, J. Chem. Phys. 0021-9606 10.1063/1.2181568 124, 154501 (2006).
42. See EPAPS Document No. E-JCPSA6-129-617827 for Appendices A and B. For more information on EPAPS, see http://www.aip.org/pubservs/epaps.html.
43. N. Bloembergen and R. V. Pound, Phys. Rev. 0031-899X 95, 8 (1954).
44. M. P. Augustine, Prog. Nucl. Magn. Reson. Spectrosc. 0079-6505 10.1016/S0079-6565(01)00037-1 40, 111 (2002).
45. A. Szöke and S. Meiboom, Phys. Rev. 0031-899X 113, 585 (1959).
46. S. Bloom, J. Appl. Phys. 0021-8979 10.1063/1.1722859 28, 800 (1957).
47. A. Vlassenbroek, J. Jeener, and P. Broekaert, J. Chem. Phys. 0021-9606 10.1063/1.470468 103, 5886 (1995).
48. X. -A. Mao and C. -H. Ye, J. Chem. Phys. 0021-9606 10.1063/1.465727 99, 7455 (1993).
49. D. Wu and C. S. Johnson, Jr., J. Magn. Reson., Ser. A 1064-1858 10.1006/jmra.1994.1192 110, 113 (1994).
50. J. Jeener, A. Vlassenbroek, and P. Broekaert, J. Chem. Phys. 0021-9606 10.1063/1.469808 103, 1309 (1995).
51. W. E. Hull, in Two-Dimensional NMR for Chemists and Biochemists, 2nd ed., edited by, W. R. Croasmun, and, R. M. K. Carlson, (VCH, New York, 1994), pp. 67-456.