Analysis of pesticides in nuts by online reversed-phase liquid chromatography-gas chromatography using the through-oven transfer adsorption/desorption interface

Journal of Agricultural and Food Chemistry

Volumn 56, Issue 14, 2008, Pages 5544-5549

  Cortés, Jose M ^a   Toledano, Rosa M ^b   Villén, Jesús ^a   Vázquez, Ana ^b  

^a UNIVERSITY OF CASTILLA LA MANCHA   (Spain)

^b Escuela Universitaria de Magisterio de Albacete   (Spain)

Author keywords

Nuts; Pesticide residue analysis; Reversed phase liquid chromatography gas chromatography (RPLC GC); TOTAD interface

Indexed keywords

ACETIC ACID DERIVATIVE; ACETIC ACID ETHYL ESTER; PESTICIDE RESIDUE; SODIUM SULFATE; SULFATE;

ARTICLE; CHEMISTRY; HAZELNUT; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METHODOLOGY; NUT; PEANUT; PISTACHIO; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SUNFLOWER; WALNUT;

ACETATES; ARACHIS HYPOGAEA; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CORYLUS; HELIANTHUS; JUGLANS; NUTS; PESTICIDE RESIDUES; PISTACIA; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SULFATES;

ARACHIS HYPOGAEA; CORYLUS; HELIANTHUS; JUGLANS; PISTACIA VERA;

EID: 49049110048     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf800773k     Document Type: Article

References (12)

1. Halvorsen, B. L.; Carlsen, M. H.; Phillips, K. M.; Bohn, S. K.; Holte, K.; Jacobs, D. R., Jr.; Blomhoff, R. Content of redox-active compounds (i.e. antioxidant) in food consumed in the United States. Am. J. Clin. Nutr. 2006, 84, 95-135.
2. Gentile, C.; Tesoriere, L.; Butera, D.; Fazzari, M.; Monastero, M.; Allegra, M.; Livrea, M. A. Antioxidant activiy of Sicilian pistachio (Pistacia ver L. var. Bronte) nut extract and its bioactive components. J. Agric. Food Chem. 2007, 55, 643-648.
3. Kocyigit, A.; Koylu, A. A.; Keles, H. Effects of pistachio nut consumption on plasma lipid profile and oxidative status in healthy volunteers. Nutr., Metab. Cardiovasc. Dis. 2006, 16, 202-209.
4. Rejeb, S. B.; Cléroux, C.; Lawrence, J. F.; Geay, P.; Wu, S.; Stavinski, S. Development and characterization of immunoaffinity columns for the selective extraction of a new developmental pesticide: Thifluzamide, from peanuts. Anal. Chim. Acta 2001, 432, 193-200.
5. Barker, S. A.; Long, A. R.; Short, C. R. Isolation of drug residues from tissues by solid-phase dispersion. J. Chromatogr. 1989, 475, 353-361.
6. Dorea, H. S.; Lanòas, F. M. Matrix solid phase extraction of organophosphorus and synthetic pyrethroid pesticides in cashew nut and passion fruit. J. Microcolumn Sep. 1999, 11, 367-375.
7. Garcinuño, R. M.; Ramos, L.; Férnandez-Hernando, P.; Cámara, C. Optimization of a matrix solid-phase dispersion method with subsequent clean-up for the determination of ethylene bisdithiocarbamate residues in almond samples. J. Chromatogr., A 2004, 1041, 35-41.
8. Husain, S. W.; Kiarostami, V.; Morrovati, M.; Tagebakhsh, M. R. Multiresidue determination of diazinon and ethion in pistachio nuts by use of matrix solid phase dispersion with a lanthanum silicate co-column and gas chromatography. Acta Chromatogr. 2003, 13, 208-214.
9. Cortés, J. M.; Sánchez, R.; Díaz-Plaza, E. M.; Villén, J.; Vázquez, A. Large volume GC injection for the analysis of organophosphorus pesticides in vegetables using the through oven transfer adsorption desorption (TOTAD) interface. J. Agric. Food Chem. 2006, 54, 1997-2002.
10. Sánchez, R.; Vázquez, A.; Andini, J. C.; Villén, J. Automated multiresidue analysis of pesticides in olive oil by on-line reversed-phase liquid chromatography-gas chromatography using the through oven transfer adsorption-desorption interface. J. Chromatogr., A 2004, 1029, 167-172.
11. Sánchez, R.; Cortés, J. M.; Villén, J.; Vázquez, A. Determination of organophosphorus and triazine pesticides in olive oil by online coupling reversed-phase liquid chromatography/gas chromatography with nitrogen-phosphorus detection and an automated through oven transfer adsorption-desorption interface. J. AOAC Int. 2005, 88, 1255-1260.
12. Díaz-Plaza, E. M.; Cortés, J. M.; Vázquez, A.; Villén, J. Automated determination of pesticide residues in olive oil by online reversed-phase liquid chromatography-gas chromatography using the through oven transfer adsorption-desorption interface with electron capture and nitrogen-phosphorus detectors operating simultaneously. J. Chromatogr., A 2007, 1174, 145-150.