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Crystal data for FH and FD was collected at T, 103.0(2) Kusing Bruker 3-circle, SMARTAPEX CCD with χ-axis fixed at 54.74°, running on SMART V 5.625 program (Bruker AXS: Madison, 2001, Graphite monochromated MoKα (λ, 0.71073 Å) radiation was employed for data collection and corrected for Lorentz and polarization effects using SAINT V 6.22 program (Bruker AXS: Madison, 2001, and reflection scaling (SADABS program, Bruker AXS: Madison, WI, 2001, Both the structures were solved by direct methods (SHELXTL 5.10, Bruker AXS: Madison, 2000) and all non-hydrogen atoms refined anisotropically using full-matrix least-squares refinement on F 2. Hydrogen atoms were added at calculated positions. For FH, Mr, 2393.46, triclinic, space group P1, a, 11.806(5, b, 12.393(5, c, 15.729(6) α, 75.073(6, β, 76.024(6, γ, 66.1515
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2 = 1.005. CCDC 608207 (FH) and 608209 (FD) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data_request/cif.
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