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The 1H NMR spectrum of [Ag6Hg312·32]12+ complex at 323 K displayed three resonances for protons a, c, and d of 1, exhibiting the relatively free rotation of the two rotors. VT 1H NMR spectra are shown in Figure S10. The formation of [Ag6Hg 312·32]12+ was also demonstrated by ESI-TOF mass spectrometry Figure S6
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In this study the synchronous helix inversions were demonstrated for the RTRs. Since the helix inversion takes place both by the ligand exchange (EX) and the flip motion (flip, if both motions take place at the same frequency, every co-occurring combination of the ligand exchange and the flip motion on both sides, that is, EX(rotor A)-EX(rotor B, EX(rotor A)-flip(rotor B, flip(rotor A)-EX(rotor B, or flip(rotor A)-flip(rotor B) is possible. In the present case, the detailed information is missing on this point
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