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Volumn 11, Issue 8, 2008, Pages 907-910

Synthesis and characterization of the highest connected 3D Wells-Dawson POM/TMC hybrid

Author keywords

Electrochemical properties; Hydrothermal synthesis; Inorganic organic hybrid; Silver; Wells Dawson polyoxometalate

Indexed keywords


EID: 46749158630     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2008.04.005     Document Type: Article
Times cited : (30)

References (37)
  • 29
    • 46749102959 scopus 로고    scopus 로고
    • note
    • 18 (6271.87): Calcd. C 14.92, H 0.99, N 2.90.
  • 30
    • 46749141396 scopus 로고    scopus 로고
    • note
    • 2. All calculations were performed using the SHELXL-97 program package. Absorption effects were empirically collected. All atoms except hydrogen atoms were refined anisotropically. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 2EZ, UK (Fax: +44 1223 336033; E-mail: deposit@ccdc.cam.ac.uk).
  • 36
    • 46749086326 scopus 로고    scopus 로고
    • note
    • Cyclic voltammograms were obtained with a CHI 660 electrochemical workstation at room temperature. Platinum gauze was used as counter electrode and Ag/AgCl electrode was referenced. A chemically bulk-modified carbon paste electrode (CPE) was used as working electrode, which was prepared as the following: 48 mg of graphite powder and 8 mg of compound 1 was mixed and ground together by agate mortar and pestle to achieve a uniform mixture, and then it was added 0.6 mL nujol with stirring. The homogenized mixture was packed into a glass tube with 1.2 mm inner diameter, and the tube surface was wiped with paper. Electrical contact was established with copper rod through the back of the electrode.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.