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46749146874
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note
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-1, KBr pellet): 3577(m), 3495(m), 2863(w), 2772(w), 2638(w), 2544(w), 1699(vs), 1606(vs), 1557(vs), 1439(s), 1397(vs), 1277(vs), 1200(s), 1117(s), 1049(vs), 896(m), 797(w), 771(m), 755(w), 696(m), 625(s), 579(w), 542(w), and 442(w).
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17
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46749148490
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note
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2 with anisotropic thermal parameters for all non-hydrogen atoms (SHELXTL Version 5.1). The coordination water molecule is disorder. All hydrogen atoms except for the hydrogen atoms bonded to disorder water oxygen were added according to theoretical models. The disorder water hydrogen atoms are not located.
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18
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0035847909
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0036129594
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14844321949
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0000966391
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34
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12844269962
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37
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46749134477
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note
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Symmetry codes: A -x + 3/2, y + 1/2, -z + 3/2; B x + 1/2, -y + 1/2, z + 1/2; C -x + 2, -y + 1, -z + 1; D - x + 1, -y + 1, -z + 1; E -x + 3/2, y + 1/2, -z + 1/2; F -x + 3/2, y - 1/2, -z + 3/2; G x - 1/2, -y + 1/2, z - 1/2; H - x + 3/2, y - 1/2, -z + 1/2.
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