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Bulk p-type BiSbTe alloy ingots were loaded into a jar with balls inside the argon-filled glove box to avoid oxidation of the nanopowder. The jar was loaded into a ball mill and processed for several hours. When the nanopowder was ready, it was loaded into 1.25- to 2.5-cm (inner diameter) dies and compacted into a 100% dense solid NC bulk sample by a hot press. Samples are available for testing upon request
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Bulk p-type BiSbTe alloy ingots were loaded into a jar with balls inside the argon-filled glove box to avoid oxidation of the nanopowder. The jar was loaded into a ball mill and processed for several hours. When the nanopowder was ready, it was loaded into 1.25- to 2.5-cm (inner diameter) dies and compacted into a 100% dense solid NC bulk sample by a hot press. Samples are available for testing upon request.
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46449111817
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We cut hot-pressed NC bulk pellets into blocks (2 mm by 3 mm by 1 mm) that were ground down into smaller blocks (2 mm by 3 mm by 0.002 mm) using a mechanical tripod polisher. We then glued the sample to a copper grid and milled it using a precision ion polishing system (Gatan Inc., Warrendale, Pennsylvania, USA) for 30 min, with incident energy of 3.2 kV and beam current of 15 μA at an incident angle of 3.5°.
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We cut hot-pressed NC bulk pellets into blocks (2 mm by 3 mm by 1 mm) that were ground down into smaller blocks (2 mm by 3 mm by 0.002 mm) using a mechanical tripod polisher. We then glued the sample to a copper grid and milled it using a precision ion polishing system (Gatan Inc., Warrendale, Pennsylvania, USA) for 30 min, with incident energy of 3.2 kV and beam current of 15 μA at an incident angle of 3.5°.
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The work is supported by the U.S. Department of Energy (DOE) grant no. DE-FG02-00ER45805 (Z.F.R.), DOE grant no. DE-FG02-02ER45977 (G.C.), NSF-Nanoscale Interdisciplinary Research Team grant no. 0506830 (G.C., Z.F.R., and M.S.D.), National Science Foundation of China project no. 50528203 (J.M.L. and Z.F.R.), and the Ministry of Science and Technology of China project no. 2006CB921802 (J.M.L.). G.C. and Z.F.R. are cofounders of GMZ Energy, Inc.
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The work is supported by the U.S. Department of Energy (DOE) grant no. DE-FG02-00ER45805 (Z.F.R.), DOE grant no. DE-FG02-02ER45977 (G.C.), NSF-Nanoscale Interdisciplinary Research Team grant no. 0506830 (G.C., Z.F.R., and M.S.D.), National Science Foundation of China project no. 50528203 (J.M.L. and Z.F.R.), and the Ministry of Science and Technology of China project no. 2006CB921802 (J.M.L.). G.C. and Z.F.R. are cofounders of GMZ Energy, Inc.
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