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42
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4644283290
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note
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Desilylation at some point in the reaction sequence thus giving 5d cannot be ruled out
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43
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4644310553
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note
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Crystallographic data (excluding structure factors) for 5d has been deposited with the Cambridge Crystallographic Data Centre as supplementary publication number CCDC 243514. Copies of the data may be obtained, free of charge, on application to CCDC, 12 Union Road, Cambridge, CB2 1EZ, UK (fax: +44(0)-1223-336033 or email: deposit@ccdc.cam.ac.uk)
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46
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48
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4644299353
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note
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2 (292 mg, 1 mmol) in THF (5 mL) was cooled to -78°C before n-BuLi (0.8 mL of a 2.5 M soln. in hexanes, 2 mmol) was added dropwise
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