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Volumn 183, Issue 6, 2008, Pages 1461-1470

Simple and high yielding synthesis of new α-aminophosphonates from imines

Author keywords

aminophosphonate; 2 Chloroquinoline 3 carbaldehyde; Imines; TMSCl; Triethylphosphite

Indexed keywords


EID: 45949100394     PISSN: 10426507     EISSN: 15635325     Source Type: Journal    
DOI: 10.1080/10426500701681532     Document Type: Article
Times cited : (21)

References (41)
  • 8
    • 0001426452 scopus 로고
    • and references cited therein;
    • (a) O. Meth-Cohn, Heterocycles, 35, 539 (1993), and references cited therein;
    • (1993) Heterocycles , vol.35 , pp. 539
    • Meth-Cohn, O.1
  • 10
    • 0003759164 scopus 로고
    • Phosphorus Containing Insecticides
    • Marcel Dekker: New York, ch. 16
    • R. Engel, Phosphorus Containing Insecticides, Handbook of Organophosphorus Chemistry (Marcel Dekker: New York, 1992), ch. 16.
    • (1992) Handbook of Organophosphorus Chemistry
    • Engel, R.1
  • 18
    • 45949092792 scopus 로고    scopus 로고
    • G. L. Drake, and T. A. Calamari, Industrial Uses of Phosphonates (Review), R. L. Hilder Brand,; Ed. (CRC Press. Boca Raton, 1983), Chap. 7.
    • G. L. Drake, and T. A. Calamari, Industrial Uses of Phosphonates (Review), R. L. Hilder Brand,; Ed. (CRC Press. Boca Raton, 1983), Chap. 7.
  • 40
    • 45949111184 scopus 로고    scopus 로고
    • Spectral data for the all the compounds are as given as follows. 3a) Diethyl (3-fluorophenylamino)(2-chloroquinolin-3-yl)methylphosphonate: IR (KBr, 3311 cm-1, NH, 1234 cm-1, P=O, 1032 cm-1(-P-O-C, 1H NMR (CDCl3, δ ppm, 1.05 (t, 3H, O-CH2-CH3, J, 8 Hz, 1.35 (t, 3H, O-CH2-CH3,J, 8 Hz, 3.7 (m, 1H, O-CH2-CH3, 3.9 (m, 1H, O-CH 2-CH3, 4.2 (m, 2H, O-CH2-CH 3, 5.4 (d, 1H, NH-CH-P=O, J, 24 Hz, 6.3-6.5 (m, 3H, Ph-H, C2,C4,C6, 7.0 (dd, 1H, Ph-H, C5,J, 8 Hz, 7.5 (t, 1H, Quinolin-H, C 5,J, 8 Hz, 7.69 (t, 1H, Quinolin-H, C6,J, 8 Hz, 7.75 (d,1H, Quinolin-H, C7,J, 8 Hz, 7.99 d, 1H, Quinolin-H, C8,J, 8 Hz, 8.34
    • 3); 5.15 (s, 1H, -CH-NH-Ph); 5.35


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.