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15
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44749089031
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note
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as(O-C-O) of oxalate anion.
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16
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44749085913
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note
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2 using full matrix least-squares methods with SHELXTL version 97 [17]. Anisotropic thermal parameters were refined for the non-hydrogen atoms, and Hydrogen atoms were theoretically added and riding on their parent atoms.
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17
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44749084223
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G.M. Sheldrick, SHELXL-97, Program for the Refinement of Crystal Structure, University of Göttingen, Germany, 1997.
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G.M. Sheldrick, SHELXL-97, Program for the Refinement of Crystal Structure, University of Göttingen, Germany, 1997.
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18
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44749090943
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note
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A pulsed Q-switched Nd:YAG laser with λ = 1064 nm was used to generate a SHG signal from samples (which was prepared into a powder pellet with ca. 150 μm diameters and ca. 0.8 mm thickness under 300 MPa pressure). The backward scattered SHG light was collected using a spherical concave mirror and passed through a filter which transmits only 532 nm radiation. The SHG efficiencies of 1 and 2 were estimated according to the principle proposed by Kurtz and Perry [20].
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20
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0642363731
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Pellaux R., Schmalle H.W., Huber R., Fischer P., Hauss T., Ouladdiaf B., and Decurtins S. Inorg. Chem. 36 (1997) 2301
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Pellaux, R.1
Schmalle, H.W.2
Huber, R.3
Fischer, P.4
Hauss, T.5
Ouladdiaf, B.6
Decurtins, S.7
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