Development and validation of HPLC method for the determination of tobramycin in urine samples post-inhalation using pre-column derivatisation with fluorescein isothiocyanate

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 869, Issue 1-2, 2008, Pages 59-66

  Mashat, M ^a   Chrystyn, H ^b   Clark, B J ^a   Assi, K H ^a  

^a UNIVERSITY OF BRADFORD   (United Kingdom)

^b Division of Pharmacy and Pharmaceutical Sciences   (United Kingdom)

Author keywords

Assay; Fluorescein isothiocyanate (FITC); HPLC; Tobramycin; Urinary pharmacokinetic; Validation

Indexed keywords

FLUORESCEIN ISOTHIOCYANATE (FITC); TOBRAMYCIN; URINARY PHARMACOKINETIC; VALIDATION;

AMINO ACIDS; BIOASSAY; BODY FLUIDS; DRUG PRODUCTS; ISOMERS; PHOTOEXCITATION;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

ACETIC ACID; ACETONITRILE; AMINE; AMINOGLYCOSIDE ANTIBIOTIC AGENT; FLUORESCEIN ISOTHIOCYANATE; METHANOL; NEOMYCIN; TOBRAMYCIN;

ACCURACY; ADULT; ANALYTIC METHOD; ARTICLE; CONCENTRATION (PARAMETERS); DERIVATIZATION; DRUG DETERMINATION; DRUG URINE LEVEL; ENVIRONMENTAL TEMPERATURE; FEMALE; HUMAN; ISOMER; MALE; NEBULIZER; NORMAL HUMAN; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SEPARATION TECHNIQUE; SOLID PHASE EXTRACTION; VALIDATION PROCESS;

ADMINISTRATION, INHALATION; ADULT; ANTI-BACTERIAL AGENTS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FEMALE; FLUORESCEIN-5-ISOTHIOCYANATE; FLUORESCEINS; FLUORESCENT DYES; HUMANS; ISOTHIOCYANATES; MALE; REPRODUCIBILITY OF RESULTS; TOBRAMYCIN;

EID: 44749086918     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2008.05.012     Document Type: Article

References (34)

1. Anhalt J.P., and Brown S.D. Clin. Chem. 24 (1978) 1940
2. Athanikar N.A., Jurgents R.W., Sturgeonl R.T., Zober A., Deluca P., and Papadimitrious D. J. Parenteral Sci. Technol. 37 (1983) 125
3. Back S.E., Nilsson-Ehle I., and Nilsson-Ehle P. Clin. Chem. 25 (1979) 1222
4. Banerjee S.K., Wells A., and Dasgupta A. Ther. Drug Monit. 21 (1999) 540
5. Barends D.M., Blauw J.S., Mijnsbergen C.W., Grovers C.J.L.R., and Hulschoof A. J. Chromatogr. 322 (1985) 321
6. Barends D.M., Brouwers J.C.A.M., and Hulschoof A. J. Pharm. Biomed. Anal. 5 (1987) 613
7. Barends D.M., Zwaan C.L., and Hulschoof A. J. Chromatogr. 225 (1981) 417
8. Brady M.S., Katz S.E., and Assoc J. Off. Anal. Chem. 70 (1987) 641
9. Charm S.E., Chi R., and Assoc J. Off. Anal. Chem. 71 (1988) 304
10. Darwish A.I. J. Pharm. Biomed. Anal. 30 (2003) 1539
11. Dash A.K., and Suryanarayanan R. J. Pharm. Biomed. Anal. 9 (1991) 237
12. Einarsson S., Folestad S., Josefsson B., and Lagerkvist S. Anal. Chem. 58 (1986) 1638
13. Essers L. J. Chromatogr. Sci. 305 (1984) 345
14. Fabre H., Sekkat M., Blanchin M., and Mandrou B. J. Pharm. Biomed. Anal. 7 (1989) 1711
15. Feng C.-H., Lin S.-J., Wu H.-L., and Chen S.-H. J. Chromatogr. B 780 (2002) 349
16. Food and Drug Administration (FDA), Center for Drug Evaluation and Research (CDER), Center for Veterinary Medicine (CVM): Guidance for Industry: Bioanalytical Method Validation, May 2001.
17. Gambardella P., Punziano R., Gionti M., Guadalupi C., Mancini G., and Mangia A. J. Chromatogr. 348 (1985) 229
18. Validation of Analytical Procedures: Methodology Q2B, ICH Steering Committee, 6 November 1996, website http://www.ich.org/.
19. Hanko V.P., and Rohrer J.S. J. Pharm. Biomed. Anal. 40 (2006) 1006-1012
20. Higgins C., and Kastner R. Antimicrob. Agents Chemother. (Bethesda) 7 (1971) 324
21. Kabra P.M., Bhatnagar P.K., Nelson M.A., Wall J.H., and Marton L.J. Clin. Chem. 29 (1983) 672
22. Keevil B.G., Lockharta S.J., and Cooperb D.P. J. Chromatogr. B 794 (2003) 329
23. Koeda T., and Umemura M.Y. In: Umezawa H., and Hooper I.R. (Eds). Aminoglycoside Antibiotics (1982), Springer-Verlag, Berlin p. 293
24. Kubo H., Kinoshita T., Kobayashi Y., and Tokunaga K. J. Liq. Chrom. Rel. Technol. 7 (1984) 2219
25. Lia F., and Sheehan T. J. Chromatogr. 609 (1992) 173
26. Maitra S., Yoshikawa T., Hansen J., Schotz M., and Guze L. Am. J. Clin. Pathol. 71 (1979) 428
27. Marples J., and Oates M.D. J. Antimicrob Chemother. 10 (1982) 311
28. Martlbauer E., Usleber E., Schneider E., and Dietrich R. Analyst 119 (1994) 2543
29. Megoulas N., and Koupparis M. Anal. Bioanal. Chem. 382 2 (2005) 290
30. Russ H., McClear D., Katimy R., Montana J., Miller R.B., Krishnamoorthy R., and Davis C.W. J. Liq. Chrom. Rel. Technol. 21 (1998) 2165
31. Stead D.A. J. Chromatogr. B 747 (2000) 69
32. Szúnyog J., Adams E., Roets E., and Hoogmartens J. J. Pharm. Biomed. Anal. 23 (2000) 891
33. Chrystyn H. Br. J. Clin. Pharmacol. 51 (2001) 289
34. Walshe M., Kelly M.T., Smyth M.R., and Ritchie H. J. Chromatogr. A 708 (1995) 31