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13C NMR (dept) spectra, and FTIR and DSC curves of the copolymers are shown in the Supporting Information.
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13C NMR (dept) spectra, and FTIR and DSC curves of the copolymers are shown in the Supporting Information.
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36
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44449138186
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The CPD incorporations were estimated on the basis of the ratio of total integration values of CPD vs ethylene at each resonance in the 13C NMR spectra. The amounts of the CPD and triads in the ethylene backbone were calculated by 13C NMR with the following equations (C, CPD and E, ethylene, EEE, ICH2/2; [EEC, CEE, 2 [ECE, ECE, I3, I4, I6, I8)/4; [CEC, /3′, I 4′)/4, where Ix is the normalized integral of peak x shown in Figure 2. On the basis of these equations, the amounts of CPD and ethylene in the copolymers were calculated as follows: [E, EEE, EEC, CEE, CEC, C, ECE, CCC, ECC, CCE, 2[CEC, Hence, the ratio of [C] to, C, E, reflected the CPD incorporation in the copolymers: CPD incorporation: CPD mol , C, C, E
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x is the normalized integral of peak x shown in Figure 2. On the basis of these equations, the amounts of CPD and ethylene in the copolymers were calculated as follows: [E] = [EEE] + [EEC + CEE] + [CEC]; [C] = [ECE] + [CCC] + [ECC + CCE] + 2[CEC]. Hence, the ratio of [C] to ([C] + [E]) reflected the CPD incorporation in the copolymers: CPD incorporation: CPD (mol %) = [C]/([C] + [E]).
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