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Crystal data for 1: C3H5Cu2N 3O2, monoclinic, space group C2/c, M r, 242.18, a, 13.7386(18) Å, b, 8.0167(10) Å, c, 7.2151(9) Å, β, 113.971(2)°, V, 726.12(16) Å3, Z, 4, Dc, 2.215 g/cm3, μ, 5.796 mm-1, F(000, 472, Tmin, 0.4574, Tmax, 0.8013, 2θmax, 54°, S, 1.190, R1, 0.0549, wR2, 0.1450. Crystal data for 2: C3H5Cu2N 3O2, monoclinic, space group P21/c, Mr, 242.18, a, 12.0108(16) Å, b, 8.3037(11) Å, c, 7.5441(10) Å, β, 95.773(2)°, V, 748.59(17) Å3, Z, 4, Dc, 2.149 g/cm3, μ, 5.622 mm
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max = 54°, S = 1.183, R1 = 0.0605, wR2 = 0.1764. CCDC Nos. 669718 and 669719.
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