[1-(2-Phenylethyl)-2,3,4,5-tetramethylcyclopentadienyl]-titanium compounds. Synthesis and their use for the syndiospecific polymerization of styrene

Organometallics

Volumn 15, Issue 23, 1996, Pages 4944-4950

  Flores, Juan C ^a,b   Wood, John S ^a   Chien, James C W ^a   Rausch, Marvin D ^a  

^a UNIVERSITY OF MASSACHUSETTS   (United States)

^b UNIVERSITY OF ALCALÁ   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 4243127001     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om960475s     Document Type: Article

References (63)

1. (a) Ishihara, N.; Seimiya, T.; Kuramoto, M.; Uoi, M. Macromolecules 1986, 19, 2464.
2. (b) Ishihara, N.; Kuramoto, M.; Uoi, M. Macromolecules 1988, 21, 3356.
3. (a) Chien, J. C. W.; Salajka, Z. J. Polym. Sci.: Part A, Polym. Chem. 1991, 29, 1253.
4. (b) Zambelli, A.; Pellecchia, C.; Oliva, L.; Longo, P.; Grassi, A. Makromol. Chem. 1991, 192, 223.
5. (c) Chien, J. C. W.; Salajka, Z.; Dong, S. Macromolecules 1992, 25, 3199.
6. (a) Kucht, A.; Kucht, H.; Barry, S.; Chien, J. C. W.; Rausch, M. D. Organometallics 1993, 12, 3075.
7. (b) Ready, T. E.; Day, R. O.; Chien, J. C. W.; Rausch, M. D. Macromolecules 1993, 26, 5822.
8. (c) Kucht, H.; Kucht, A.; Chien, J. C. W.; Rausch, M. D. Appl. Organomet. Chem. 1994, 8, 393.
9. (a) Jordan, R. F.; Bajgur, C. S.; Willett, R.; Scott, B. J. Am. Chem. Soc. 1986, 108, 7410.
10. (b) Jordan, R. F. Adv. Organomet. Chem. 1991, 32, 325.
11. (a) Chien, J. C. W.; Tsai, W.-M.; Rausch, M. D. J. Am. Chem. Soc. 1991, 773, 8570.
12. (b) Tsai, W.-M.; Rausch, M. D.; Chien, J. C. W. Appl. Organomet. Chem. 1993, 7, 71.
13. (c) Elder, M. J.; Razavi, A.; Ewen, J. A. U.S. Patents 5,155,080 (Oct 13, 1992) and 5,225,500 (July 6, 1993) (to Fina Technology, Inc.).
14. (d) For a recent review see: Möhring, P. C.; Coville, N. J. J. Organomet. Chem. 1994, 479, 1.
15. (a) Marks, T. J. Acc. Chem. Res. 1992, 25, 57.
16. (b) Bochmann, M.; Lancaster, S. J. Angew. Chem., Int. Ed. Engl. 1994, 33, 1634.
17. (a) Gillis, D. J.; Tudoret, M.-J.; Baird, M. C. J. Am. Chem. Soc. 1993, 115, 2543.
18. (b) Wang, Q.; Quyoum, R.; Gillis, D. J.; Tudoret, M.-J.; Jeremic, D.; Hunter, B. K.; Baird, M. C. Organometallics 1996, 15, 693.
19. (c) Pellecchia, C.; Immirzi, A.; Zambelli, A. J. Organomet. Chem. 1994, 479, C9.
20. (d) Pellecchia, C.; Immirzi, A.; Pappalardo, D.; Peluso, A. Organometallics 1994, 13, 3773.
21. (e) Pellecchia, C.; Immirzi, A.; Grassi, A.; Zambelli, A. Organometallics 1993, 12, 4473.
22. (f) Pellecchia, C.; Grassi, A.; Immirzi, A. J. Am. Chem. Soc. 1993, 115, 1160.
23. (g) Lancaster, S. J.; Robinson, O. B.; Bochmann, M. Organometallics 1995, 14, 2456.
24. (a) Reference 3c.
25. (b) Pellecchia, C.; Longo, P.; Proto, A.; Zambelli, A. Makromol. Chem., Rapid Commun. 1992, 13, 265.
26. (c) Pellecchia, C.; Proto, A.; Longo, P.; Zambelli, A. Makromol. Chem., Rapid Commun. 1992, 13, 277.
27. (d) Campbell, R. E. (Dow Chemical Co.) Int. Pat. Appl. WO 93/03,067 (Chem. Abstr. 1993, 119, 204155b); U.S. Pat. Appl. 5,066,741, continuation of Eur. Pat. Appl. Ep 421,659 (Chem. Abstr. 1991, 115, 72440j).
28. (d) Campbell, R. E. (Dow Chemical Co.) Int. Pat. Appl. WO 93/03,067 (Chem. Abstr. 1993, 119, 204155b); U.S. Pat. Appl. 5,066,741, continuation of Eur. Pat. Appl. Ep 421,659 (Chem. Abstr. 1991, 115, 72440j).
29. (e) Pellecchia, C.; Pappalardo, D.; Oliva, L.; Zambelli, A. J. Am. Chem. Soc. 1995, 117, 6593.
30. (a) Grassi, A.; Pellecchia, C.; Oliva, L. Macromol. Chem. Phys. 1995, 196, 1093.
31. (b) Grassi, A.; Zambelli, A.; Laschi, F. Organometallics 1996, 15, 480.
32. (a) Ogasa, M.; Mallin, D. T.; Macomber, D. W.; Rausch, M. D.; Rogers, R. D.; Rollins, A. N. J. Organomet. Chem. 1991, 405, 41.
33. (b) Siemeling, U. J. Chem. Soc., Chem. Commun. 1992, 1335.
34. (c) Hughes, A. K.; Meetsma, A.; Teuben, J. H. Organometallics 1993, 12, 1936.
35. (d) Wang, T.-F.; Lee, T.-Y.; Chou, J.-W.; Ong, C.-W. J. Organomet. Chem. 1992, 423, 31.
36. (e) Wang, T.-F.; Wen, Y.-S. J. Organomet. Chem. 1992, 439, 155.
37. (f) Jutzi, P.; Dahinaus, J.; Kristen, M. D. J. Organomet. Chem. 1993, 450, C1.
38. (g) Jutzi, P.; Kristen, M. D.; Dahlhaus, J.; Newmann, B.; Stammler, H.-G. Organometallics 1993, 12, 2980.
39. (h) Herrmann, W. A.; Morawietz, M. J. A.; Priermeier, T.; Mashima, K. J. Organomet. Chem. 1995, 486, 291.
40. (h) Okuda, J,; du Plooy, K. E.; Toscano, P. J. J. Organomet. Chem. 1995, 495, 195.
41. Qichen, H.; Yanlong, Q.; Guisheng, L.; Youqi, T. Trans. Met. Chem. 1990, 15, 48.
42. (a) Flores, J. C.; Chien, J. C. W.; Rausch, M. D. Organometallics 1994, 13, 4140.
43. (b) Flores, J. C.; Chien, J. C. W.; Rausch, M. D. Macromolecules, in press.
44. Nadasdi, T. T.; Huang, Y.; Stephan, D. W. Inorg. Chem. 1993, 32, 347.
45. Zimmermann, K. H.; Pilato, R. S.; Horváth, I. T.; Okuda, J. Organometallics 1992, 11, 3935.
46. (b) Okuda, J.; Zimmermann, K. H. Chem. Ber. 1992, 125, 637 and references therein.
47. Okuda, J.; Zimmermann, K. H. J. Organomet. Chem. 1988, 344, C1.
48. Jutzi, P.; Dahlhaus, J. Synthesis 1993, 7, 684.
49. (a) Jutzi, P. Chem. Rev. 1986, 86, 983.
50. (b) Dahlhaus, J.; Bangel, M.; Jutzi, P. J. Organomet. Chem. 1994, 474, 55.
51. (a) Horton, A. D.; Frijns, J. H. G. Angew. Chem., Int. Ed. Engl. 1991, 30, 1152.
52. (b) Solari, E.; Floriani, C.; Chiesi-Villa, A.; Guastini, C. J. Chem. Soc., Chem. Commun. 1989, 1747.
53. Bochmann, M.; Karger, G.; Jaggar, A. J. J. Chem. Soc., Chem. Commun. 1990, 1038.
54. For a discussion see: Reference 10c and literature cited therein.
55. Blanco, S. G.; Gómez-Sal, P.; Carreras, S. M.; Mena, M.; Royo, P.; Serrano, R. J. Chem. Soc., Chem. Commun. 1986, 1572.
56. (a) Reference 2b.
57. (b) Longo, P.; Proto, A.; Zambelli, A. Macromol. Chem. Phys. 1995, 196, 3015 and references therein.
58. Perrin, D. P.; Armarego, W. L. F. Purification of Laboratory Chemicals, 3rd ed.; Pergamon Press Ltd.: Oxford, U.K., 1988.
59. Llinas, G. H.; Dong, S.-H.; Mallin, D. T.; Rausch, M. D.; Lin, Y.-G.; Winter, H. H.; Chien, J. C. W. Macromolecules 1992, 25, 1242.
60. Sheldrick, G. M. SHELX-TL; Structure determination and full matrix least squares refinements program package, 1988.
61. International Tables for X-ray Crystallography; Kynoch Press: Birmingham, U.K., 1974; Vol. IV, pp 99, 149.
62. Stewart, R. F.; Davidson, R. F.; Simpson, W. J. J. Chem. Phys. 1965, 42, 3175.
63. Cromeri D. T.; Liberman, D. J. J. Chem. Phys. 1970, 53, 1891.