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Volumn 37, Issue 3, 2008, Pages 282-283

Temperature dependence of refractive index of films of well-defined linear and star-shaped polystyrenes

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EID: 42049116817 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2008.282 Document Type: Article

Times cited : (10)

References (7)

1
- 0003520107
- Gakkaisyuppan Center, Tokyo
- For example: In Refractive-index Control of Transparent High Polymers, Gakkaisyuppan Center, Tokyo, 1998.
- (1998) Refractive-index Control of Transparent High Polymers

2
- 0004278335
- Elsevier Applied Science, London
- G. H. Meeten, Optical Properties of Polymers, Elsevier Applied Science, London, 1989.
- (1989) Optical Properties of Polymers
- Meeten, G.H.¹

3
- 33646254396
- H. Kudo, H. Inoue, T. Nishikubo, T. Anada, Polym. J. 2006, 38, 289.
- (2006) Polym. J , vol.38 , pp. 289
- Kudo, H.¹ Inoue, H.² Nishikubo, T.³ Anada, T.⁴

4
- 0006278227
- For example: a
- For example: a) J. Wang, K. Matyjaszewski, J. Am. Chem. Soc. 1995, 111, 5614.
- (1995) J. Am. Chem. Soc , vol.111 , pp. 5614
- Wang, J.¹ Matyjaszewski, K.²

5
- 0030148869
- b) T. E. Patten, J. Xia, T. Abernathy, K. Matyjaszewski, Science 1996, 272, 866.
- (1996) Science , vol.272 , pp. 866
- Patten, T.E.¹ Xia, J.² Abernathy, T.³ Matyjaszewski, K.⁴

6
- 42049123189
- 2-), 1.84-2.05 (m, 30H, >CH-), 6.46-7.24 (m, 154H, aromatic H).
- 2-), 1.84-2.05 (m, 30H, >CH-), 6.46-7.24 (m, 154H, aromatic H).

7
- 42049093940
- A typical procedure for the synthesis of star-shaped polySTs was as follows (Run 6 in Table 1, The reaction of CRA-BP (0.022 g, 0.0125 mmol, CuBr (0.015g, 0.1 mmol, bipyridine (0.032 g, 0.2 mmol, and ST (1.04 g, 10 mmol) was carried out in DMF (1.2 mL) at 130 °C for 2 h in vacuo in a polymerization tube. After that, CHCl3 was added to the resulting mixture and the whole was washed with water several times. The organic layer was evaporated and poured into a large amount of n-hexane to precipitate the star-shaped polyST as a white solid. IR (film, cm-1, 1750 (v C=O ester, 1595 and 1490 (v C=C aromatic, 1HNMR (500 MHz, CDCl 3, TMS) δ 0.50-1.53 (m, 412H, CH3 of calixarene, C(O)-C(CH3)2, and -CH2, 1.86-2.06 (m, 176H, >CH, 4.50 (broad s, 4.0H, >CH- of calixarene, 6.46-7.24 m, 888H, aromatic H
- 2-), 1.86-2.06 (m, 176H, >CH-), 4.50 (broad s, 4.0H, >CH- of calixarene), 6.46-7.24 (m, 888H, aromatic H).

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