One-step purification of 3,4-dihydroxyphenyllactic acid, salvianolic acid B, and protocatechualdehyde from Salvia miltiorrhiza bunge by isocratic stepwise hydrogen bond adsorption chromatography on cross-linked 12% agarose

Journal of Chromatographic Science

Volumn 46, Issue 2, 2008, Pages 165-168

  Gu, M ^a   Su, Z G ^a   Janson, J C ^b  

^a INSTITUTE OF PROCESS ENGINEERING   (China)

^b UPPSALA UNIVERSITY   (Sweden)

Author keywords

[No Author keywords available]

Indexed keywords

SALVIA MILTIORRHIZA;

EID: 40949102777     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/46.2.165     Document Type: Article

References (19)

1. Y.R. Lu and L.Y. Foo. Polyphenols of Salvia - a review. Phytochemistry 59: 117-140 (2002).
2. G.C. Lin and W.L. Chang. Diterpenoids from Salvia miltiorrhiza. Phytochemistry 53: 951-953 (2000).
3. C.T. Wu, V. Mulabagal, S.M. Nalawade, C.L. Chen, T.F. Yang, and H.S. Tsay. Isolation and quantitative analysis of cryptotanshinone, an active quinoid diterpene formed in callus of Salvia miltiorrhiza Bunge. Biol. Pharm. Bull. 26: 845-848 (2003).
4. J.P. Yuan, H. Chen, and F. Chen. Simultaneous determination of rosmarinic acid, lithospermic acid B, and related phenolics in Salvia miltiorrhiza by HPLC. J. Agric. Food Chem. 46: 2651-2654 (1998).
5. M. Petersen and M.S.J. Simmonds. Rosmarinic acid. Phytochemistry 62: 121-125 (2003).
6. Y.H. Lin, A.H. Liu, H.L. Wu, C. Westernbroek, Q.L. Song, H.M. Yu, G.J.T. Horst, and X.J. Li. Salvianolic acid B, an antioxidant from Salviamiltiorrhiza, prevents Ab25-35-induced reduction in BPRP in PC12 cells. Biochem. Biophys. Res. Commun. 348: 593-599 (2006).
7. Z.P. Wang, J.Y. FAN, Y.Q. Liu, and Y.J. Yuan. Study on compare between ethanol disposal and resin adsorption technique from radix Danshen. Ion Exchange and Adsorption 19: 554-560 (2003).
8. J. Pan and T. Xu. Preparative separation of D(+)-8-(3,4-dihydrophenyl)- lactate sodium from Salvia miltiorrhiza by HPLC, Chinese Traditional and Herbal Drugs 34: 125-127 (2003).
9. H.B. Li, J.P. Lai, Y. Jiang, and F. Chen. Preparative isolation and purification of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by high-speed counter-current chromatography. J. Chromatogr., A 943: 235-239 (2002).
10. J.H. Chen, F.M. Wang, F.S.C. Lee, X.R. Wang, and M.Y. Xie. Separation and identification of water-soluble salvianolic acids from Salvia miltiorrhiza Bunge by high-speed counter-current chromatography and ESI-MS analysis. Talanta 69: 172-179 (2006).
11. W.B. Zhi and Q.Y. Deng. Purification of salvianolic acid B from the crude extract of Salvia miltiorrhiza with hydrophilic organic/salt-containing aqueous two-phase system by counter-current chromatography. J. Chromatogr., A 1116: 149-152(2006).
12. J. Xu, T. Tan, and J.-C. Janson. One-step simultaneous purification of three water-soluble bio-active constituents in crude extracts from radix of Danshen (Salviae miltiorrhiza) by adsorption chromatography on oligo-β-cyclodextrin substituted agarose gel media. Proc. Biochem. 42: 480-485 (2007).
13. M. Gu, Z.-G. Su, and J.-C. Janson. The separation of polyphenols by isocratic hydrogen bond adsorption chromatography on a cross-linked 12% agarose gel. Chromatographia 64: 247-253 (2006).
14. M.A. Ruttenberg, T.P. King, and L.C. Craig. The chemistry of Tyrocidine. VI. The amino acid sequence of Tyrocidine C. Biochemistry 4: 11-18 (1965).
15. D. Eaker and J. Porath. Sorption effects in gel filtration. I. A survey of amino acid behaviour on Sephadex G-10. Sep. Sci. 2: 507-521 (1967).
16. J.-C. Janson. Adsorption phenomena on Sephadex. J. Chromatogr. 28: 12-20 (1967).
17. M. Gu, Z.-G. Su, and J.-C. Janson. One-step purification of resveratrol and polydatin from Polygonum cuspidatum (Sieb. & Zucc.) by isocratic hydrogen-bond adsorption chromatography on cross-linked 12% agarose. Chromatographia 64: 701-704 (2006).
18. T. Andersson, M. Carlsson, L. Hagel, P.-Å. Pernemalm, and J.-C. Janson. Agarose-based media for high-resolution gel filtration of biopolymers. J. Chromatogr. 326: 33-44 (1985).
19. P.-A. Pernemalm, M. Carlsson, G. Lindgren. U.S. Patent 4665164 (1987).