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Crystallographic data for the complex: C30H32N 2CuO6, Mr, 580.14, monoclinic, space group P2/n (No. 13, a, 14.50(4, b, 11.36(2, c, 18.43(4) Å, β, 107.93(3)°, V, 2889(12)Å3, Z, 4, Dcalcd 1.334gcm-3, μ(MoKα, 0.800 mm -1, T, 293 K, λ, 0.7107 Å, ω scan, 21272 reflections measured, 5870 unique, R, 0.0869 all data, The data collection was performed on a Rigaku CCDC Mercury system. The structure was solved by a direct method using SIR-92 and refined on F2. Geometrical hydrogen atoms were located on the calculated positions. All non-hydrogen atoms were treated anisotropically. Hydrogen atoms were included but not refined. Crystallographic data reported in this paper has been deposited with Cambridge Crystallographic Data Centre as supplementary pub
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2. Geometrical hydrogen atoms were located on the calculated positions. All non-hydrogen atoms were treated anisotropically. Hydrogen atoms were included but not refined. Crystallographic data reported in this paper has been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-xxxx.
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14
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38949206756
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Crystallographic data for the complex: C26H20N 2CuO4, Mr, 488.00, monoclinic, space group P2/n (No. 13, a, 9.826(6, b, 15.11(3, c, 15.174(9) Å, β, 93.01(2)°, V, 2249(5)Å3, Z, 4, Dcalcd 1.441gcm-3, μ(MoKα, 1.007 mm -1, T, 293 K, λ, 0.7107 Å, ω scan, 13826 reflection measured, 5854 unique, R, 0.0850 all data, The data collection was performed on a Rigaku CCDC Mercury system. The structure was solved by a direct method using SIR-92 and refined on F2. Geometrical hydrogen atoms were located on the calculated positions. All non-hydrogen atoms were treated anisotropically. Hydrogen atoms were included but not refined. Crystallographic data reported in this paper have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-xxxx
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2. Geometrical hydrogen atoms were located on the calculated positions. All non-hydrogen atoms were treated anisotropically. Hydrogen atoms were included but not refined. Crystallographic data reported in this paper have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-xxxx.
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38949138645
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Supporting Information is available electronically on the CSJ-Journal web site;
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Supporting Information is available electronically on the CSJ-Journal web site; http://www.csj.jp/journals/chem-lett/.
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