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38549174198
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note
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-1): 490(m), 657(m), 962(m), 1072(m), 1226(m), 1358(s), 1525(s), 1636(m), 2855(w), 2970(w), 3180(m), 3430(w).
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34
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38549147584
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note
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2 by full-matrix least-squares using SHELXTL97 [35]. All non-hydrogen atoms were refined with anisotropic displacement parameters.
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35
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38549134506
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G.M. Sheldrick, SHELXTL, Crystallographic Software Package, Version 5.1, Bruker-AXS, Madison, WI, 1998.
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G.M. Sheldrick, SHELXTL, Crystallographic Software Package, Version 5.1, Bruker-AXS, Madison, WI, 1998.
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