Detection and quantification of provitamin D2 and vitamin D 2 in hop (Humulus lupulus L.) by liquid chromatography-diode array detection-electrospray ionization tandem mass spectrometry

Journal of Agricultural and Food Chemistry

Volumn 55, Issue 20, 2007, Pages 7995-8002

  Magalhães, Paulo J ^a   Carvalho, Daniel O ^a   Guido, Luís F ^a   Barros, Aquiles A ^a  

^a UNIVERSITY OF PORTO   (Portugal)

Author keywords

Ergocalciferol; Ergosterol; Hop; HPLC DAD; HPLC MS MS; Sterols; Vitamin D

Indexed keywords

HUMULUS; HUMULUS LUPULUS;

ERGOCALCIFEROL; ERGOSTEROL;

ARTICLE; CHEMISTRY; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMULUS; METHODOLOGY; QUALITY CONTROL;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; ERGOCALCIFEROLS; ERGOSTEROL; HUMULUS; QUALITY CONTROL; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

EID: 38349018750     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf071308d     Document Type: Article

References (22)

1. Magalhães, P. J.; Guido, L. F.; Cruz, J. M.; Barros, A. A. Analysis of xanthohumol and isoxanthohumol in different hop products by liquid chromatography-diode array detection-electrospray ionization tandem mass spectrometry. J. Chromatogr., A 2007, 1150, 295-301.
2. Phalip, V.; Hatsch, D.; Laugel, B.; Jeltsch, J., An overview of fungal community diversity in diseased hop plantations. FEMS Microbiol. Ecol. 2006, 56, 321-329.
3. Callemien, D.; Jerkovic, V.; Rozenberg, R.; Collin, S. Hop as an interesting source of resveratrol for brewers: optimization of the extraction and quantitative study by liquid chromatography/ atmospheric pressure chemical ionization tandem mass spectrometry. J. Agric. Food Chem. 2005, 53, 424-429.
4. Hough, J. S.; Briggs, D. E.; Stevens, R.; Young, T. W. Hops. In Malting and Brewing Science: Hopped Wort and Beer, 2nd ed.; Chapman & Hall: London, 1982; Vol. 2, pp 389-420.
5. Gül, M. K.; Amar, S. J. Sterols and the phytosterol content in oilseed rape (Brassica napus L.). Cell Mol. Biol. 2006, 5, 71-79.
6. Headley, J. V.; Peru, K. M.; Verma, B.; Robarts, R. D. Mass spectrometric determination of ergosterol in a prairie natural wetland. J. Chromatogr., A 2002, 958, 149-156.
7. Steven, A.; Warner, D. F.; Eierman, G.; Wayne, S.; Aristotle, J.D. Cycloartenol-derived sterol biosynthesis in the Peronosporales. Proc. Natl Acad. Sci. 1982, 79, 3769-3772.
8. Kadakal, C.; Nas, S.; Ekinci, R. Ergosterol as a new quality parameter together with patulin in raw apple juice produced from decayed apples. Food Chem. 2005, 90, 95-100.
9. Nissinen, M.; Gylling, H.; Vuoristo, M.; Miettinen, T. Micellar distribution of cholesterol and phytosterols after duodenal plant stanol ester infusion. Am. J. Physiol. Gastrointest. Liver Physiol. 2002, 282, 1009-1015.
10. Oehrl, L.; Hansen, A.; Rohrer, C.; Fenner, G.; Boyd, C. Oxidation of phytosterols in a test food system. J. Am. Oil Chem. Soc 2001, 78, 1073-1078.
11. 2 by UV radiation. Food Chem. 2005, 92, 541-546.
12. Eitenmiller, R. R.; Landen, W. O. Vitamin D. In Vitamin Analysis for the Health and Food Sciences; CRC Press: New York, 1998; p 77.
13. Toh, T. H.; Prior, B. A.; Van der Merwe, M. J. Quantification of plasma membrane ergosterol of Saccharomyces cerevisiae by direct-injection atmospheric pressure chemical ionization/tandem mass spectrometry. Anal. Biochem. 2001, 288, 44-51.
14. Varga, M.; Bartók, T.; Mesterházy, A. Determination of ergosterol in Fusarium-infected wheat by liquid chromatography-atmospheric pressure photoionization mass spectrometry. J. Chromatogr., A 2006, 1103, 278-283.
15. Perales, S.; Alegría, A.; Barberá, R.; Farré, R. Determination of vitamin D in dairy products by high-performance liquid chromatography. Food Sci. Technol. Int. 2005, 11, 451-462.
16. Seitz, L. M.; Mohr, H. E.; Burroughs, R.; Sauer, B. Ergosterol as an indicator of fungal invasion in grains. Cereal Chem. 1977, 54, 1207-1217.
17. Kurmann, A.; Indyck, H. The endogenous vitamin D content of bovine milk: influence of season. Food Chem. 1994, 50, 75-81.
18. Renken, S. A.; Warthensen, J. J. Vitamin D stability in milk. J. Food Sci. 1993, 58, 552-556.
19. American Chemical Society (ACS) Committee on Environmental Improvement and Subcommittee on Environmental Analytical Chemistry. Guidelines for data acquisition and data quality evaluation in environmental chemistry. Anal. Chem. 1980, 52, 2242-2249.
20. Srzednicki, G.; Craske, J.; Nimmuntavin, C.; Mantais, L. G.; Wattananon, S. Determination of ergosterol in paddy rice using solid phase extraction. J. Sci. Food Agric. 2004, 84, 2041-2046.
21. Gessner, M. O.; Schmitt, A. L. Use of solid-phase extraction to determine ergosterol concentrations in plant tissue colonized by fungi. Appl. Environ. Microbiol. 1996, 62, 415-419.
22. 2 content in edible mushrooms. J. Agric. Food Chem. 1998, 46, 5269-5272.