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Volumn 36, Issue 12, 2007, Pages 1452-1453

One-dimensional structure consisting of pin-wheel Cu4Gd core and Na+ as connector

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EID: 38149089426 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.1452 Document Type: Article

Times cited : (2)

References (16)

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14
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- Na[CuL)4Gd, A methanolic solution (30 mL) of Na[CuL]· 1.33H2O (0.13g, 0.4mmol) was gently poured into a methanolic solution (10mL) of Gd(hfac)3(H2O)2 (0.81 g, 0.1 mmol) at ambient temperature. The resulting solution was allowed to stand for several days, during which time blue-purple crystals precipitated, and they are collected by suction filtration. Crystals easily loose the crystal solvents, and the elemental analysis agrees with the formula of Na[(CuL)4Gd, Yield: 0.09g (67, IR cm-1, vc=o 1655; Vc=N 1596. Anal. Caled for C36H44N8O 16NaCu4Gd: C, 33.80; H, 3.47; N, 8.76, Found: C, 33.85; H, 3.62; N, 9.04
- 4Gd: C, 33.80; H, 3.47; N, 8.76%. Found: C, 33.85; H, 3.62; N, 9.04%.

15
- 38149126891
- A crystal with a small amount of mother liquid was encapsulated into a glass tube, and the X-ray diffraction data were collected. Crystal data for Na[(CuL)4Gd]·3H2O·2MeOH: formula C 38H58NgO21NaCu4Gd, M r, 1397.34, monoclinic, space group P21/c a =14.035(3, b, 14.766(3, c, 26.088(6) Å, β, 94.59(1)°, V, 5389(2)Å3, Z, 4; d calcd, 1.722Mg/m3; μ, 2.857 mm-1; T, 296K; R, 0.0451, wR, 0.1242. Crystallography data deposit number CCDC 663223
- -1; T = 296K; R = 0.0451, wR = 0.1242. Crystallography data deposit number CCDC 663223.

16
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